• 专利标题:   Preparation of aminated reduced graphene oxide/manganese oxide composite material for capacitor materials, heating mixture of e.g. p-phenylenediamine and dimethylformamide, and mixing with potassium permanganate aqueous solution.
  • 专利号:   CN108172408-A
  • 发明人:   CHEN X, LIU J, ZHAO W, WU Y
  • 专利权人:   UNIV HEFEI TECHNOLOGY
  • 国际专利分类:   B82Y030/00, B82Y040/00, H01G011/24, H01G011/30, H01G011/36, H01G011/46
  • 专利详细信息:   CN108172408-A 15 Jun 2018 H01G-011/24 201852 Pages: 7 Chinese
  • 申请详细信息:   CN108172408-A CN11446382 27 Dec 2017
  • 优先权号:   CN11446382

▎ 摘  要

NOVELTY - Preparation of aminated reduced graphene oxide/manganese oxide composite material involves preparing graphite oxide by Hummers method, preparing graphite oxide into an aqueous solution, stirring with dimethylformamide in a water bath at 30-40 degrees C for 1-1.5 hours, adding p-phenylenediamine solution, heating to 70-90 degrees C, stirring mixture under reflux for 9-11 hours, washing with ethanol and deionized water until the supernatant is colorlessly neutral, dispersing obtained precipitate in deionized water to obtain 0.1-1 g/L, preferably 0.5-1 g/L aminated reduced graphene oxide, ultrasonically mixing with potassium permanganate aqueous solution using hydrothermal method and transferring into a reaction vessel. USE - Preparation of aminated reduced graphene oxide/manganese oxide composite material used for preparing capacitor materials (all claimed). ADVANTAGE - The method uses aminated graphene which effectively improves the conductivity of manganese dioxide, electrochemical activity of composite material, and wettability of the material with electrolyte. The method regulates and controls the microstructure of manganese dioxide, and increases the specific surface area, thus improving the dispersibility of the composite material. The capacitor material prepared using the composite material has improved performance.