• 专利标题:   Preparation of graphene/titanium dioxide compound light catalyst used for, e.g. solar cell, by subjecting graphite oxide and organic solvent to ultrasonic processing, adding precursor of titanium salt and deionized water, and heating.
  • 专利号:   CN101890344-A, CN101890344-B
  • 发明人:   ZHU Y, YANG X, WANG S, JIANG X, ZHOU K
  • 专利权人:   UNIV EAST CHINA SCI TECHNOLOGY
  • 国际专利分类:   B01J021/06, B01J021/18
  • 专利详细信息:   CN101890344-A 24 Nov 2010 B01J-021/18 201122 Pages: 8 Chinese
  • 申请详细信息:   CN101890344-A CN10237588 27 Jul 2010
  • 优先权号:   CN10237588

▎ 摘  要

NOVELTY - A graphene/titanium dioxide compound light catalyst is prepared by dissolving graphite oxide in organic solvent, subjecting mixture to ultrasonic processing, adding a precursor of a titanium salt, stirring, adding deionized water, stirring, heating the mixture, adding absolute ethyl alcohol and deionized water, stirring, and drying. USE - Method of preparing graphene/titanium dioxide compound light catalyst for environment protection or solar cell. ADVANTAGE - The method utilizes easy to obtain raw materials, prepares product having good catalytic activity and optical property, and is simple, safe and low cost. DETAILED DESCRIPTION - A graphene/titanium dioxide compound light catalyst is prepared by: (A) dissolving graphite oxide (5-60 g) in organic solvent (20-50 ml), and subjecting mixture to ultrasonic processing for 30-60 minutes to obtain dispersion solution; (B) adding a precursor of a titanium salt into the dispersion solution, stirring for 20-60 minutes, adding deionized water (0-1 ml), and stirring for 30-90 minutes; and (C) heating the mixture at 120-200 degrees C for 4-20 hours, adding absolute ethyl alcohol and deionized water, stirring, and drying at 40-80 degrees C for 8-24 hours. The organic solvent is absolute ethyl alcohol, isopropyl alcohol, ethylene glycol, and/or ethanol-acetic acid. The precursor of the titanium salt is titanium tetrachloride, tetrabutyl titanate, or titanium tetraisopropanolate. The ratio of graphite oxide and precursor of the titanium salt is 1:10-500