• 专利标题:   Preparing polyamide-amine dendritic macromolecules/nano-graphene composite material involves adding carboxylated graphene to deionized water, and then stirring obtained mixture.
  • 专利号:   CN105148995-A, CN105148995-B
  • 发明人:   PENG X, TANG X, LI Z
  • 专利权人:   UNIV JISHOU
  • 国际专利分类:   B01J031/06, C02F001/74, C02F101/38
  • 专利详细信息:   CN105148995-A 16 Dec 2015 B01J-031/06 201630 Pages: 6 English
  • 申请详细信息:   CN105148995-A CN10607953 23 Sep 2015
  • 优先权号:   CN10607953

▎ 摘  要

NOVELTY - Preparing polyamide-amine dendritic macromolecules/nano-graphene composite material involves adding 0.42g carboxylated graphene to 40mL deionized water, and then stirring obtained mixture at 40 degrees C for 4 hours. The solution is filtered, centrifuged and washed with deionized water. Polyamide-amine dendritic macromolecules are added to washed material, and stirred at 35 degrees C to obtain a mixture. The mixture is washed with deionized water, and then dried to obtain a mixed product. Cobalt(II) chloride and sodium borohydride are added to mixed product, and then stirred at 50 degrees C for 4 hours. USE - Method for preparing polyamide-amine dendritic macromolecules/nano-graphene composite material (claimed). ADVANTAGE - The method enables to prepare polyamide-amine dendritic macromolecules/nano-graphene composite material in an eco-friendly manner. DETAILED DESCRIPTION - Preparing polyamide-amine dendritic macromolecules/nano-graphene composite material involves adding 0.42g carboxylated graphene to 40mL deionized water, and then stirring obtained mixture at 40 degrees C for 4 hours. The solution is filtered, centrifuged and washed with deionized water. Polyamide-amine dendritic macromolecules are added to washed material, and stirred at 35 degrees C to obtain a mixture. The mixture is washed with deionized water, and then dried to obtain a mixed product. Cobalt(II) chloride and sodium borohydride are added to mixed product, and then stirred at 50 degrees C for 4 hours. The obtained product is washed with deionized water. The obtained product is centrifuged, and then washed with deionized water. The washed material is dried in presence of vacuum to obtain the desired product.