• 专利标题:   Self-crosslinking thiophene-based graphene dispersant useful for preparing nano-carbon material dispersion liquid, comprises e.g. 9-(thiophen-2-ylmethyl)-5,13-dioxa-9-aza-1,17-disilaheptadecan-1,1,1,7,11,17,17,17-octol.
  • 专利号:   CN115322214-A
  • 发明人:   XIONG Y, GAO J, YU H, FENG X, CHEN X, GUO L, CUI J
  • 专利权人:   UNIV LIAONING
  • 国际专利分类:   C01B032/15, C01B032/174, C01B032/194, C07F007/08
  • 专利详细信息:   CN115322214-A 11 Nov 2022 C07F-007/08 202312 Chinese
  • 申请详细信息:   CN115322214-A CN10874451 25 Jul 2022
  • 优先权号:   CN10874451

▎ 摘  要

NOVELTY - Self-crosslinking thiophene-based graphene dispersant, comprises DSiTP i.e. 9-(thiophen-2-ylmethyl)-5,13-dioxa-9-aza-1,17-disilaheptadecan-1,1,1,7,11,17,17,17-octol (I). USE - The self-crosslinking thiophene-based graphene dispersant is useful for preparing nano-carbon material dispersion liquid (claimed). ADVANTAGE - The self-crosslinking thiophene-based graphene dispersant has a simple preparation process, high dispersion efficiency, and utilizes nano-carbon material dispersion liquid which can be stored for a long time. DETAILED DESCRIPTION - Self-crosslinking thiophene-based graphene dispersant, comprises DSiTP i.e. 9-(thiophen-2-ylmethyl)-5,13-dioxa-9-aza-1,17-disilaheptadecan-1,1,1,7,11,17,17,17-octol of formula (I). INDEPENDENT CLAIMS are also included for: Preparing self-crosslinking thiophene-based graphene dispersant, comprising (i) taking a certain amount of thiophene-2-methylamine and 3-glycidyloxypropyltrimethoxysilane in methanol reagent, stirring and reacting for a period of time under a nitrogen atmosphere and a certain temperature, after reacting, evaporating to remove methanol to obtain dispersant precursor, and (ii) taking a certain amount of dispersant precursor, adding to a certain concentration of formic acid aqueous solution, stirring and reacting for a certain time under a nitrogen atmosphere and a certain temperature to obtain final product; and Preparing nano-carbon material dispersion liquid, comprising taking a certain mass of nano-carbon material powder, adding self-crosslinking thiophene-based graphene dispersant, and deionized water, ultrasonicating in a water bath, and then ultrasonically dispersing by ultrasonic cell crusher to obtain final product.