• 专利标题:   Preparing graphene conductive composite fiber involves adding 3-amino propyl triethoxy silane, ethanol sequentially added to distilled water, adjusting temperature and stirring, adding graphene, and performing high speed centrifugal treatment.
  • 专利号:   CN115233330-A
  • 发明人:   WANG X, LUO Q, LI P
  • 专利权人:   UNIV JIAXING NANHU
  • 国际专利分类:   D01F001/09, D01F001/10, D01F006/52
  • 专利详细信息:   CN115233330-A 25 Oct 2022 D01F-006/52 202308 Chinese
  • 申请详细信息:   CN115233330-A CN10918397 01 Aug 2022
  • 优先权号:   CN10918397

▎ 摘  要

NOVELTY - Preparing graphene conductive composite fiber by: adding 3-amino propyl triethoxysilane and ethanol sequentially to distilled water, adjusting the temperature to 55℃, stirring for 15 minutes, adding graphene, performing ultrasonic treatment for 30-40 minutes to obtain a mixed suspension; performing high speed centrifugal treatment, filtering to obtain reactant; washing and drying to obtain modified graphene; mixing modified graphene with oxidizing liquid, carrying out oxidation treatment to obtain the modified oxidation graphene; dispersing modified oxidized graphene in ethyl acetate to prepare a modified graphene dispersion liquid; adding acrylic acid, modified rosin to ethyl acetate, preparing acrylic acid mixed solution; adding modified graphene dispersion liquid into acrylic acid mixed solution, stirring to obtain spinning stock solution; extruding stock solution, spraying thin stream of stock solution through needle into a coagulation bath, and precipitating. USE - Preparation graphene of conductive composite fiber used in special occasion in antistatic clothes or electromagnetic radiation-proof clothes. Uses include but are not limited to electric heating and anti-electromagnetic radiation function. ADVANTAGE - The conductive composite fiber prepared by the method has excellent conductivity and mechanical property, has high conductivity, fiber strength, and average conductivity of more than 6 S/cm.