• 专利标题:   Preparing porous zinc cobaltate-graphene composition active material/foam nickel super capacitor electrode comprises e.g. mixing graphene oxide and block polymer surfactant P123, dispersing ultrasonically in aqueous urea solution.
  • 专利号:   CN107492451-A
  • 发明人:   GAO Z, ZHANG L, WU D, XU F, WANG Z, JIANG K
  • 专利权人:   UNIV HENAN NORMAL
  • 国际专利分类:   H01G011/24, H01G011/26, H01G011/28, H01G011/30, H01G011/36, H01G011/46, H01G011/86
  • 专利详细信息:   CN107492451-A 19 Dec 2017 H01G-011/24 201811 Pages: 7 Chinese
  • 申请详细信息:   CN107492451-A CN10651058 02 Aug 2017
  • 优先权号:   CN10651058

▎ 摘  要

NOVELTY - Preparing porous zinc cobaltate-graphene composition active material/foam nickel super capacitor electrode comprises e.g. mixing graphene oxide and block polymer surfactant P123, dispersing ultrasonically in an aqueous urea solution to form a uniform dispersion, adding cobalt nitrate and zinc acetate to the dispersion to form a uniform precursor solution, transferring precursor to hydrothermal reactor, adding foam nickel into hydrothermal reactor precursor solution, carrying out hydrothermal reaction in nickel foam current collector deposited on surface of cobalt-zinc hydroxide-graphene. USE - The method is useful for preparing porous zinc cobaltate-graphene composition active material/foam nickel super capacitor electrode (claimed). ADVANTAGE - The method is simple, easy to control, economical and produces high-performance super-capacitor in a larger scale. DETAILED DESCRIPTION - Preparing porous zinc cobaltate-graphene composition active material/foam nickel super capacitor electrode comprises mixing graphene oxide and block polymer surfactant P123, dispersing ultrasonically in an aqueous urea solution to form a uniform dispersion, adding cobalt nitrate and zinc acetate to the dispersion to form a uniform precursor solution, transferring precursor solution to hydrothermal reactor, adding foam nickel into hydrothermal reactor precursor solution, carrying out hydrothermal reaction at 90-150 degrees C in nickel foam current collector deposited on surface of cobalt-zinc hydroxide-graphene composition, ultrasonically washing and drying, transferring to muffle furnace, calcining at 250 degrees C in air atmosphere.