• 专利标题:   Preparing composite material used for manufacturing metal material, by stirring mixed solution made of graphene and aluminum powder, adding aluminum-silicon-copper alloy, melting, pouring into mold, smelting, casting, aging, and cooling.
  • 专利号:   CN112962001-A
  • 发明人:   YAN H, XIONG J
  • 专利权人:   UNIV NANCHANG
  • 国际专利分类:   B22D023/00, B22F003/14, C22C001/06, C22C001/10, C22C021/02, C22F001/02, C22F001/043
  • 专利详细信息:   CN112962001-A 15 Jun 2021 C22C-001/10 202161 Pages: 9 Chinese
  • 申请详细信息:   CN112962001-A CN10030613 11 Jan 2021
  • 优先权号:   CN10030613

▎ 摘  要

NOVELTY - Preparing graphene-reinforced aluminum-based composite material involves: (1) ultrasonically dispersing and mixing graphene and aluminum powder to obtain a mixed solution; (2) magnetically stirring the mixed solution, drying, sintering to obtain an aluminum graphene intermediate prefabricated block, cutting into small particles, and wrapping with an aluminum foil; (3) cutting aluminum-silicon-copper base alloy into small pieces, adding to a graphite crucible, heating, heat-preserving, melting the base alloy, then adding small particles of block to the crucible at different angles, cooling the melt, and pouring into a mold to obtain a molten cast blank; (4) adding the blank to a vacuum melting furnace for smelting, spraying, and casting to obtain a casting blank; and (5) adding the blank to a vacuum heat treatment furnace for solution treatment (A), heat-preserving, cooling, adding to the furnace for solution treatment (B), heat-preserving, cooling, aging, and cooling. USE - The method is useful for preparing graphene-reinforced aluminum-based composite material used for manufacturing metal material. ADVANTAGE - The method enables stable, safe and environmentally-friendly preparation of composite material, which has high performance characteristics and mechanical property, and uniform distribution. DETAILED DESCRIPTION - Preparing graphene-reinforced aluminum-based composite material involves: (1) ultrasonically dispersing and mixing graphene and aluminum powder to obtain a mixed solution; (2) magnetically stirring the mixed solution by using a thermostatic heating magnetic stirrer, drying in a vacuum drying oven, sintering in a vacuum hot-press sintering furnace to obtain an aluminum graphene intermediate prefabricated block, cutting into small particles, and wrapping with an aluminum foil; (3) cutting aluminum-silicon-copper base alloy into small pieces, adding to a graphite crucible, placing in a resistance furnace, heating at 780-800 degrees C, heat-preserving for 25-30 minutes, melting the base alloy, then adding small particles of block to the crucible at different angles, applying high-energy ultrasonic wave while adding block, quickly cooling the melt, and pouring into a mold to obtain a molten cast blank; (4) adding the blank to a vacuum melting furnace for smelting, spraying, and casting to obtain a casting blank; and (5) adding the blank to a vacuum heat treatment furnace for solution treatment (A) at 510 plus minus 5 degrees C, heat-preserving for 3.5-4.5 hours, quickly adding to water at 50-60 degrees C to cool, adding to the furnace for solution treatment (B) at 530 plus minus 5 degrees C, heat-preserving 4-5 hours, cooling, aging at 180 plus minus 5 degrees C for 9-10 hours, and cooling.