• 专利标题:   Preparation of graphene-based carbon paper used in manufacture of e.g. capacitor, involves mixing concentrated sulfuric acid and nitric acid, soaking graphite paper in obtained electrolyte, electrochemically oxidizing, and drying.
  • 专利号:   CN104261387-A, CN104261387-B
  • 发明人:   LU X, TONG Y, YU M, WANG W, CENG Y
  • 专利权人:   UNIV SUN YATSEN
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN104261387-A 07 Jan 2015 C01B-031/04 201518 Pages: 7 Chinese
  • 申请详细信息:   CN104261387-A CN10470758 16 Sep 2014
  • 优先权号:   CN10470758

▎ 摘  要

NOVELTY - Preparation of graphene-based carbon paper involves mixing concentrated sulfuric acid and concentrated nitric acid in ratio of 10-20 mL:10-20 mL, soaking a graphite paper in obtained mixed electrolyte, electrochemically oxidizing at 13-17 V for 15-35 minutes, washing resultant paper, drying, and placing obtained graphene oxide carbon paper in hydrazine hydrate to reduce. The ratio of graphite sheet and mixed electrolyte is 1-3 g:20-40 mL. USE - Preparation of graphene-based carbon paper used in manufacture of capacitor and lithium battery material (all claimed), and used as electrode material of supercapacitor. ADVANTAGE - The method enables preparation of graphene-based carbon paper with high graphene surface area.