• 专利标题:   Preparing graphene film electrode involves dissolving graphene oxide solid in water by ultrasonic dispersion treatment to obtain graphene oxide dispersion, and placing the graphene oxide dispersion vacuum filtration apparatus.
  • 专利号:   CN105575679-A, CN105575679-B
  • 发明人:   FANG J
  • 专利权人:   FUZHOU DUOWEI CARBON ENVIRONMENTAL TECHN, FUJIAN SHAOWU YONGFEI CHEM CO LTD
  • 国际专利分类:   C01B031/04, H01G011/36, H01G011/86, C01B032/19
  • 专利详细信息:   CN105575679-A 11 May 2016 H01G-011/86 201659 Pages: 15 English
  • 申请详细信息:   CN105575679-A CN10960028 18 Dec 2015
  • 优先权号:   CN10960028

▎ 摘  要

NOVELTY - Preparing graphene film electrode involves dissolving graphene oxide solid in water by ultrasonic dispersion treatment to obtain 1-2mg/ml graphene oxide dispersion, and placing the graphene oxide dispersion vacuum filtration apparatus to obtain graphene oxide film. The pH value of graphene oxide dispersion is adjusted to 9-11. Areducing agent is added to graphene oxide dispersion, and then stirred at 80-95 degrees C for 1-6 hours. The obtained product is washed with pure water to remove excess reducing agent and accelerator. The washed product is dried to give solid graphene. USE - Method for preparing graphene film electrode (claimed). ADVANTAGE - The method increases performance of graphene film electrode. DETAILED DESCRIPTION - Preparing graphene film electrode involves dissolving graphene oxide solid in water by ultrasonic dispersion treatment to obtain 1-2mg/ml graphene oxide dispersion, and placing the graphene oxide dispersion vacuum filtration apparatus to obtain graphene oxide film. The pH value of graphene oxide dispersion is adjusted to 9-11. Areducing agent is added to graphene oxide dispersion, and then stirred at 80-95 degrees C for 1-6 hours. The obtained product is washed with pure water to remove excess reducing agent and accelerator. The washed product is dried to give solid graphene. The graphene solid is dissolved in 100ml pure water by ultrasonic dispersion treatment to obtain graphene dispersion. Proppant is added to graphene dispersion, and then ultrasonically dispersed to obtain graphene mixture. The graphene mixture is poured into a vacuum filtration apparatus, where the mixture is processed to obtain graphene oxide/graphene composite membrane. The graphene oxide/graphene composite membrane is treated at room temperature, and then immersed in an aqueous hydrogen iodide solution. The graphene oxide/graphene composite membrane is dried at 80-95 degrees C for 0.5-3 hours, and then processed at room temperature to obtain graphene film electrode.