• 专利标题:   Preparing molybdenum disulfide/nickel sulfide-graphene composite sheet used in electrode materials, involves dispersing graphene oxide uniformly in deionized water to obtain graphene oxide suspension, adding sodium molybdate and thiourea.
  • 专利号:   CN105655140-A, CN105655140-B
  • 发明人:   LIU A, ZHAO L, WU H, ZHANG J, YIN Z
  • 专利权人:   UNIV ZHEJIANG SCITECH
  • 国际专利分类:   H01G011/24, H01G011/30, H01G011/86, H01M010/0525, H01M004/36
  • 专利详细信息:   CN105655140-A 08 Jun 2016 H01G-011/24 201664 Pages: 9 Chinese
  • 申请详细信息:   CN105655140-A CN10128453 07 Mar 2016
  • 优先权号:   CN10128453

▎ 摘  要

NOVELTY - Preparing molybdenum disulfide/nickel sulfide chip, involves dispersing graphene oxide uniformly in deionized water to obtain graphene oxide suspension. Sodium molybdate, nickel chloride and thiourea are added in graphene oxide suspension and ultrasonic treatment is performed to give a mixed solution. ethylene glycol is added to the mixed solution, transferred to the reaction vessel and hydrothermally reacted at 160-200 degrees C to obtain a black product. The black product is washed with ethanol and vacuum dried at 80 degrees C to obtain sheet-like molybdenum disulfide/nickel sulfide-graphene composite. USE - Method for preparing molybdenum disulfide/nickel sulfide-graphene composite sheet (claimed) which can be used in electrode materials such as super capacitors and lithium ion batteries. ADVANTAGE - The method is simple. DETAILED DESCRIPTION - Preparing molybdenum disulfide/nickel sulfide chip, involves dispersing graphene oxide uniformly in deionized water to obtain graphene oxide suspension. Sodium molybdate (Na2MoO.2H2O), nickel chloride (NiCl2.6H2O) and thiourea (CS(NH2)2) are added in graphene oxide suspension and ultrasonic treatment is performed to give a mixed solution. The ethylene glycol is added to the mixed solution, transferred to the reaction vessel and hydrothermally reacted at 160-200 degrees C to obtain a black product. The black product is washed with ethanol and vacuum dried at 80 degrees C to obtain sheet-like molybdenum disulfide/nickel sulfide-graphene composite.