• 专利标题:   Preparing high quality water-soluble graphene comprises mixing, placing elactrodes, performing an electrolytic reaction, removing, performing ultrasonic treatment, centrifugally washing and ultrasonically mixing.
  • 专利号:   CN108821268-A
  • 发明人:   HAN L, ZHONG Y, ZHENG C
  • 专利权人:   QINGDAO OLEFINIC CARBON RUIER NEW MATERIAL TECHNOLOGY CO LTD
  • 国际专利分类:   C01B032/19
  • 专利详细信息:   CN108821268-A 16 Nov 2018 C01B-032/19 201910 Pages: 11 Chinese
  • 申请详细信息:   CN108821268-A CN10692136 20 Jun 2018
  • 优先权号:   CN10692136

▎ 摘  要

NOVELTY - Preparing high quality water-soluble graphene comprises (i) mixing aromatic carboxylic acid and metal hydroxide in deionized water, taking graphite material as anode material, a platinum sheet as a cathode material, placing the two electrodes vertically and parallelly in the electrolyte, separating distance between the two electrodes, connecting the two electrodes to a direct current stabilized voltage power supply; (ii) turning on the power supply voltage, performing an electrolytic reaction to achieve the electrochemistry peeling of anode material to obtain primary water-soluble dispersion; (iii) removing the electrode from primary water-soluble dispersion to obtain dispersion, performing ultrasonic treatment in sequence, centrifugally washing to obtain a high solids graphene slurry; and (iv) ultrasonically mixing the high solid graphene slurry in water. USE - The method is useful for preparing high quality water-soluble graphene (claimed). ADVANTAGE - The method is simple, economical, non-polluting, highly efficient and the graphene has good electrical, thermal conductivity and mechanical properties.