• 专利标题:   Preparing foam graphene-loaded nickel-cobalt-oxygen anode material in lithium ion battery, involves treating nickel foam and immersing it in graphene oxide solution and coating foam in solution and reducing with reducing agent.
  • 专利号:   CN108023071-A
  • 发明人:   HE D, WU X, ZHANG F, DUAN L, LI M, JIN C
  • 专利权人:   NAT ENG RES CENT NANOTECHNOLOGY
  • 国际专利分类:   H01M004/36, H01M004/52, H01M010/0525
  • 专利详细信息:   CN108023071-A 11 May 2018 H01M-004/36 201835 Pages: 5 Chinese
  • 申请详细信息:   CN108023071-A CN11214847 28 Nov 2017
  • 优先权号:   CN11214847

▎ 摘  要

NOVELTY - Preparing foam graphene-loaded nickel-cobalt-oxygen anode material, involves treating nickel foam and immersing it in graphene oxide solution and coating foam in solution. The graphene oxide on nickel is chemically reduced with reducing agent. The foamed nickel coated with graphene is placed in a solution, and etched by acid, and corresponding cobalt salt in molar amount of 1:2. The solution is transferred to a 100 milliliter hydrothermal reaction kettle and reacted at 160-180 degrees C for 3-5 hours, after temperature is reduced to room temperature. USE - Preparing foam graphene-loaded nickel-cobalt-oxygen anode material in lithium ion battery (claimed). ADVANTAGE - The method enables to prepare foam graphene-loaded nickel-cobalt-oxygen anode material which has large specific surface area and improves electrochemical performance of material. It's preparation process is simple and easy to operate. DETAILED DESCRIPTION - Preparing foam graphene-loaded nickel-cobalt-oxygen anode material involves treating nickel foam and immersing it in graphene oxide solution and coating foam in solution. The graphene oxide on nickel is chemically reduced with reducing agent. The foamed nickel coated with graphene is placed in a solution, and etched by acid, and corresponding cobalt salt in molar amount of 1:2. The solution is transferred to a 100 milliliter hydrothermal reaction kettle and reacted at 160-180 degrees C for 3-5 hours, after temperature is reduced to room temperature. The precipitate is vacuum-filtered and washed multiple times with ethanol. The vacuum oven is dried at 60-80 degrees C for 10-15 hours. The precipitate is calcined at 500-600 degrees C for 3-5 hours to obtain foam graphene loaded with nickel-cobalt-oxygen.