• 专利标题:   Preparation of zero-valent iron loaded on graphene hollow nanosphere nanomaterial by preparing silica-graphene oxide nanosphere, adding to nano-zero-valent iron dispersion system, stirring, ultrasonicating, centrifuging, and vacuum drying.
  • 专利号:   CN113304749-A
  • 发明人:   WU Q, SUN M, GU Q, ZHANG Y, ZHANG J, GUO W, WU H
  • 专利权人:   CHINESE ACAD SCI GUANGZHOU CHEM RES INST, GUANGDONG ACAD SCI MICROBIOLOGY INST
  • 国际专利分类:   B01J021/18, B01J023/745, B01J035/02, B01J035/10, B01J037/06, C01B032/198, C01B033/18, C02F001/72, C02F101/34, C02F101/38
  • 专利详细信息:   CN113304749-A 27 Aug 2021 B01J-023/745 202188 Pages: 12 Chinese
  • 申请详细信息:   CN113304749-A CN10427636 21 Apr 2021
  • 优先权号:   CN10427636

▎ 摘  要

NOVELTY - Preparation of zero-valent iron loaded on graphene hollow nanosphere nanomaterial comprises selecting silica nanosphere and graphene oxide, mixing in deionized water, water bath ultrasonicating for 6-48 hours, centrifuging, and vacuum drying to obtain silica-graphene oxide nanosphere; dispersing nano-zero-valent iron in deionized water to obtain first dispersion system, adding silica-graphene oxide nanosphere and reducing agent, stirring, water bath ultrasonicating for 6-8 hours, centrifuging, and vacuum drying to obtain silica-graphene oxide/zero-valent iron nanosphere; and curing to 300-400 degrees C for 6-24 hours under nitrogen atmosphere, adding to silicon oxide etchant, etching silicon oxide template, centrifuging, and vacuum drying. USE - The method is for preparation of zero-valent iron loaded on graphene hollow nanosphere nanomaterial. ADVANTAGE - The nanomaterial can effectively prevent the zero-valent iron nanomaterial from agglomerating themselves and being corroded during the catalytic degradation of N-nitrosodimethylamine, and has very large specific surface area and very high electronic conductivity which helps to exert the catalytic degradation activity of zero-valent iron nanomaterial on the by-product N-nitrosodimethylamine of disinfection, and improved reproducible degradation efficiency. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for a zero-valent iron loaded on graphene hollow nanosphere nanomaterial.