• 专利标题:   Preparation of oxidized graphene inorganic nano-phase change material by dissolving graphene oxide in distilled water, ultrasonic dispersing oxidized graphene aqueous solution, sealing, heating, and sealing.
  • 专利号:   CN106928906-A, CN106928906-B
  • 发明人:   XIAO L, ZHAO M, HU H
  • 专利权人:   UNIV JILIN CONSTR, UNIV JILIN JIANZHU
  • 国际专利分类:   C09K005/06
  • 专利详细信息:   CN106928906-A 07 Jul 2017 C09K-005/06 201757 Pages: 8 Chinese
  • 申请详细信息:   CN106928906-A CN10298512 02 May 2017
  • 优先权号:   CN10298512

▎ 摘  要

NOVELTY - Preparation of oxidized graphene inorganic nano-phase change material includes dissolving the graphene oxide in distilled water, low temperature ultrasonic dispersing, dispersion forming concentration, oxidized graphene aqueous solution, and sealing; adding sodium acetate trihydrate with potassium chloride, after heating, mixing with main heat agent; adding sodium carboxymethyl cellulose, and cutting; and ultrasonically dispersing graphene oxide aqueous solution in water bath, stirring uniformly and sealing the container to obtain the product. USE - Method for preparing oxidized graphene inorganic nano-phase change material (claimed). ADVANTAGE - The method is simple, environment-friendly and easy to operate, and has uniform and stable product property, small toxic and side effect. DETAILED DESCRIPTION - Preparation of oxidized graphene inorganic nano-phase change material comprises: (A) dissolving the graphene oxide in distilled water, low temperature ultrasonic dispersing for 120-150 minutes, dispersion forming concentration is 0.006-0.02 g/ml, oxidized graphene aqueous solution, and sealing; (B) adding 80-90 pts. wt. sodium acetate trihydrate with 2-10 pts. wt. potassium chloride, after heating, mixing with main heat agent at 80 degrees C, its phase change temperature interval is 40-50 degrees C, and main phase change enthalpy is 180-190 J/g at 15 degrees C; (C) adding 1-8 pts. wt. sodium carboxymethyl cellulose in step (B), and cutting at high speed under the condition of stirring uniformly; and (D) ultrasonically dispersing 0.1-0.5 pts. wt. graphene oxide aqueous solution in water bath, stirring uniformly and sealing the container to obtain the product.