• 专利标题:   Preparation of chlorine-doped glucose carbon-based graphene involves mixing glucose and hydrochloric acid, heating, mixing deionized water and absolute ethanol, filtering and spin-coating chlorine-doped precursor solution on quartz plate.
  • 专利号:   CN108911524-A
  • 发明人:   YU J, ZHAN X, TANG L, LIU Z
  • 专利权人:   UNIV KUNMING SCI TECHNOLOGY
  • 国际专利分类:   C03C017/22, C01B032/184
  • 专利详细信息:   CN108911524-A 30 Nov 2018 C03C-017/22 201901 Pages: 10 Chinese
  • 申请详细信息:   CN108911524-A CN10999643 30 Aug 2018
  • 优先权号:   CN10999643

▎ 摘  要

NOVELTY - The preparation of chlorine-doped glucose carbon-based graphene involves (1) mixing glucose and hydrochloric acid at mass ratio of (9-3):1 to obtain mixed solution, heating at 100-200 degrees C until the solution viscosity is 1x 105-1x 106 centipoise, mixing deionized water, absolute ethanol and prepared caramel solution at volume ratio of 1:1:(2-3) and filtering to obtain chlorine-doped precursor solution as filtrate, (2) spin-coating chlorine-doped precursor solution on quartz plate, carrying out coating process for 3 seconds at rate of 1000-1500 r/second and spinning at 2200-2800 r/second for 1 minute to obtain spin smear, (3) drying spin smear at constant temperature for 20-35 minutes, placing the dried spin smear under vacuum and annealing at 600-800 degrees C for 20-24 hours. USE - Preparation of chlorine-doped glucose carbon-based graphene. ADVANTAGE - The method enables preparation of chlorine-doped glucose carbon-based graphene ensuring controllable doping amount and large sample piece diameter by simple, economical, efficient and environmentally-friendly process.