▎ 摘　　要

NOVELTY - The preparation method of molybdenum disulfide/reduced graphite oxide composite structure powder involves (1) selecting sodium molybdate dihydrate and thiourea as reactant, and graphene oxide as a precursor, fully mixing, and uniformly dispersing to obtain suspension mixed solution, (2) hydro-thermally reacting the mixed solution in high pressure reaction vessel as reactant to prepare mixed solution of reduced graphite oxide loaded molybdenum disulfide composite structure, and (3) cleaning and drying the mixed solution. USE - Preparation of molybdenum disulfide/reduced graphite oxide composite structure powder (claimed). ADVANTAGE - The method enables preparation of molybdenum disulfide/reduced graphite oxide composite structure powder with excellent degree of crystallinity, increased adsorption of organic pollutant, excellent photocatalytic properties, and photocatalytic degradation efficiency of organic dye.