• 专利标题:   Growing carbon nanotubes on porous nano-porous copper-graphene compound involves preparing nano porous copper catalyst, cleaning copper alloy, drying copper alloy, and then keeping obtained copper alloy in hydrochloric acid solution.
  • 专利号:   CN105645376-A, CN105645376-B
  • 发明人:   KANG J, LI J, ZHANG Z, ZHANG X, ZOU C
  • 专利权人:   UNIV TIANJIN POLYTECHNIC
  • 国际专利分类:   B01J023/72, B01J035/10, B82Y030/00, C01B031/02, C01B031/04, C01B032/16, C01B032/184
  • 专利详细信息:   CN105645376-A 08 Jun 2016 C01B-031/02 201658 Pages: 10 Chinese
  • 申请详细信息:   CN105645376-A CN10967606 17 Dec 2015
  • 优先权号:   CN10967606

▎ 摘  要

NOVELTY - Growing carbon nanotubes on a porous nano-porous copper-graphene compound involves preparing nano porous copper catalyst. The copper alloy is cleaned, and then dried. The obtained copper alloy is kept in a 0.05mol/l hydrochloric acid solution. The obtained copper alloy is washed with deionized water. The obtained washed product is kept in a vacuum drying box. The obtained dried product is kept in a furnace with prepared nano porous copper catalyst. the temperature of the furnace is raised at 600-800 degrees C. USE - Method for growing carbon nanotubes on a porous nano-porous copper-graphene compound (claimed). DETAILED DESCRIPTION - Growing carbon nanotubes on a porous nano-porous copper-graphene compound involves preparing nano porous copper catalyst. The copper alloy is cleaned, and then dried. The obtained copper alloy is kept in a 0.05mol/l hydrochloric acid solution. The obtained copper alloy is washed with deionized water. The obtained washed product is kept in a vacuum drying box. The obtained dried product is kept in a furnace with prepared nano porous copper catalyst. the temperature of the furnace is raised at 600-800 degrees C. The obtained product is annealed for 2-4 hours by introducing acetylene, hydrogen and mixed gas of argon gas. The obtained product is cooled.