• 专利标题:   Method for preparing oxidized graphene quantum dot, involves mixing oxidized graphene aqueous solution, hydrogen peroxide aqueous solution and ferric ion solution followed by oxidizing mixed solution to prepare graphene quantum dot.
  • 专利号:   CN102336404-A, CN102336404-B
  • 发明人:   GUO S, ZHOU X
  • 专利权人:   UNIV SHANGHAI JIAOTONG
  • 国际专利分类:   B82Y040/00, C01B031/04
  • 专利详细信息:   CN102336404-A 01 Feb 2012 C01B-031/04 201243 Pages: 7 Chinese
  • 申请详细信息:   CN102336404-A CN10202165 19 Jul 2011
  • 优先权号:   CN10202165

▎ 摘  要

NOVELTY - An oxidized graphene quantum dot preparation method involves dispersing oxidized graphite into deionized water. The oxidized graphite is peeled-off and dispersed into a single layer for obtaining the single-layer oxidized graphene aqueous solution. The single-layer oxidized graphene aqueous solution, hydrogen peroxide aqueous solution and ferric ion solution are mixed at room temperature according to volume ratio of 5:20:0-0.5. The mixed solution is obtained and photo-catalytically oxidized for 15 minutes to 10 hours using an UV lamp to prepare the oxidized graphene quantum dot. USE - Method for preparing oxidized graphene quantum dot. ADVANTAGE - The method enables preparing the oxidized graphene quantum dot in a simple and convenient manner with even size. DETAILED DESCRIPTION - An oxidized graphene quantum dot preparation method involves dispersing oxidized graphite into deionized water for 1 hour under ultrasonic action with working frequency of 40 kHz and power of 160 W. The oxidized graphite is peeled off and dispersed into a single layer for obtaining the single-layer oxidized graphene aqueous solution. The single-layer oxidized graphene aqueous solution, hydrogen peroxide aqueous solution and ferric ion solution are mixed at room temperature according to volume ratio of 5:20:0-0.5. The mixed solution is obtained and photo-catalytically oxidized for 15 minutes to 10 hours using an UV lamp to prepare the oxidized graphene quantum dot. DESCRIPTION OF DRAWING(S) - The drawing shows a photograph of oxidized graphene quantum dot.