• 专利标题:   Preparing functional graphene carbon film material comprises e.g. using nanocellulose, dopamine, sodium alginate, theanine, and/or tannic acid as solute, adding to solvent, heat treating, adding nanosheet composition, pressurizing graphene oxide macroscopic body and pretreating graphene oxide film.
  • 专利号:   CN115259141-A
  • 发明人:   XU J, YANG C, REN Z
  • 专利权人:   AECC BEIJING AERONAUTICAL MATERIALS INST
  • 国际专利分类:   C01B032/05, C01B032/184, C01B032/194, H01B005/14, H05K007/20, H05K009/00
  • 专利详细信息:   CN115259141-A 01 Nov 2022 C01B-032/184 202302 Chinese
  • 申请详细信息:   CN115259141-A CN10653599 10 Jun 2022
  • 优先权号:   CN10653599

▎ 摘  要

NOVELTY - Preparing functional graphene carbon film material comprises (i) using nanocellulose, dopamine, sodium alginate, theanine, and/or tannic acid as a solute, and adding to a solvent to obtain a solution X1; (ii) mixing graphene oxide nanosheets a1 and reduced graphene oxide nanosheets a2, heat treating at 1000-2200℃, obtaining reduced graphene oxide nanosheets a2 from graphene oxide nanosheets for 60-300 minures under the condition of argon or nitrogen; (iii) adding the nanosheet composition to part of the solution X1, preparing a dispersion X2, and X3, mixing, and removing air bubbles and volatiles to obtain a graphene oxide dispersion; (iv) placing graphene oxide dispersion at -196℃ to 0℃, heat preserving for 30-180 minutes, and drying to remove solvent to prepare graphene oxide macroscopic bodies; (v) pressurizing graphene oxide macroscopic body; and (vi) pretreating graphene oxide film at 100-550℃ or under vacuum conditions, and heat treating. USE - The method is useful for preparing functional graphene carbon film material. ADVANTAGE - The material solves the problems of low volume density, small thermal diffusivity, and poor electrical properties of existing graphene film products. The method solves the problem of small size of graphene film products, reduces the difficulty of the process of graphene film products, and improves its production efficiency. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for functional graphene carbon film material prepared by the above method.