• 专利标题:   Preparation of high quality graphene involves dispersing crystalline flake graphite in concentrated sulfuric acid, adding potassium permanganate, deionized water, and hydrogen peroxide, stir-reacting, centrifuging, dispersing, and drying.
  • 专利号:   CN105197918-A
  • 发明人:   JIANG M, PENG S, KOU Z, ZHAO X, LI Y
  • 专利权人:   UNIV HUBEI TECHNOLOGY
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN105197918-A 30 Dec 2015 C01B-031/04 201630 Pages: 9 English
  • 申请详细信息:   CN105197918-A CN10654427 12 Oct 2015
  • 优先权号:   CN10654427

▎ 摘  要

NOVELTY - Preparation of high quality graphene comprises dispersing crystalline flake graphite in concentrated sulfuric acid and ultrasonically stirring; adding with potassium permanganate, ultrasonically stirring, and reacting at 30-50 degrees C for 0.5-2 hours and 80-100 degrees C for 1-3 hours; adding deionized water, reacting at 80-100 degrees C, stirring for 15 minutes, adding hydrogen peroxide, and stirring; and centrifuging, ultrasonically dispersing precipitate in dilute hydrochloric acid, centrifuging, ultrasonically dispersing precipitate in hydroiodic acid, repeating process, and vacuum drying. USE - Method for preparing high quality graphene (claimed). ADVANTAGE - The method avoids long oxidation time problem and is quick and efficient. DETAILED DESCRIPTION - Preparation of high quality graphene comprises dispersing crystalline flake graphite in concentrated sulfuric acid and ultrasonically stirring at 0-20 degrees C for 0.5-2 hours; adding with potassium permanganate, ultrasonically stirring at 0-20 degrees C for 0.5-2 hours, and reacting at 30-50 degrees C for 0.5-2 hours and 80-100 degrees C for 1-3 hours; adding deionized water, reacting at 80-100 degrees C, ultrasonically stirring for 15 minutes, adding hydrogen peroxide, and ultrasonically stirring; and centrifuging, ultrasonically dispersing precipitate in dilute hydrochloric acid, centrifuging, ultrasonically dispersing precipitate in hydroiodic acid, repeating process for 2 times, and vacuum drying.