• 专利标题:   Preparing niobium-based metal oxide mesoporous carbon ball composite material with oxygen defect in developing practical sodium ion battery and material of related energy storing and converting field, involves preparing niobium pentachloride ethanol solution.
  • 专利号:   CN114300665-A
  • 发明人:   SHUI L, WANG X, MA C, LUO D
  • 专利权人:   UNIV SOUTH CHINA NORMAL
  • 国际专利分类:   C01B032/05, C01G033/00, H01M010/054, H01M004/36, H01M004/48, H01M004/583
  • 专利详细信息:   CN114300665-A 08 Apr 2022 H01M-004/36 202242 Chinese
  • 申请详细信息:   CN114300665-A CN11649183 30 Dec 2021
  • 优先权号:   CN11649183

▎ 摘  要

NOVELTY - Preparing niobium-based metal oxide mesoporous carbon ball composite material with oxygen defect involves preparing niobium pentachloride ethanol solution, ultrasonically mixing uniformly to obtain solution A, adding the solution A into the mesoporous carbon ball, ultrasonically soaking to obtain precursor B. The obtained precursor B is placed in a vacuum oven to dry, placed the dried sample in a tubular furnace filled with hydrogen argon mixed gas, sintered at 450-750degrees Celsius, cooled to room temperature to obtain product represented as niobium oxide-x MEC, where the range of x is 0.1-0.5, and the volume ratio of the hydrogen is 5-20%. USE - Method for preparing niobium-based metal oxide mesoporous carbon ball composite material with oxygen defect used in developing the practical sodium ion battery and the material of the related energy storing and converting field. ADVANTAGE - 0.1-10:1,The method realizes the multiplying power performance of the 20A g-1 over 5000 times of the over-long circulating service life. DETAILED DESCRIPTION - INDEPENDENT CLAIMS are included for the following: 1. Sodium ion cathode material, comprises niobium-based metal oxide mesoporous carbon ball composite material with oxygen defect and 2. Sodium ion battery, comprises negative electrode made of the sodium ion cathode material.