• 专利标题:   Purification of graphene oxide involves encapsulating graphene oxide dispersion in synthetic organic polymer fabric bag, subjecting to dialyzed cleaning, and freeze-drying high-purity graphene oxide solution.
  • 专利号:   CN104692365-A
  • 发明人:   XUE Q, YANG J, YAN X
  • 专利权人:   LANZHOU CHEM PHYSICS INST CHINESE ACAD
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN104692365-A 10 Jun 2015 C01B-031/04 201566 Chinese
  • 申请详细信息:   CN104692365-A CN10651625 06 Dec 2013
  • 优先权号:   CN10651625

▎ 摘  要

NOVELTY - High-acidity graphite oxide solution is uniformly stirred in deionized water, and aqueous phase containing graphite oxide is separated. Oxidized graphite is washed and ultrasonically dispersed to obtain graphene oxide dispersion. Obtained dispersion is encapsulated in synthetic organic polymer fabric bag and subjected to dialyzed cleaning process, to obtain high-purity graphene oxide solution. The concentration of graphite oxide in the organic polymer synthetic fabric bag dilute solution is 0.5-20 mg/ml. Obtained graphene oxide solution is freeze-dried to obtain graphene oxide powder. USE - Purification of graphene oxide (claimed). ADVANTAGE - The method efficiently and economically provides purified graphene oxide, by simple method. DETAILED DESCRIPTION - High-acidity graphite oxide solution having pH of 0.5-1, is uniformly stirred in deionized water, and aqueous phase containing graphite oxide is separated. The upper aqueous phase then is removed, stirred with deionized water, and oxidized graphite is washed and ultrasonically dispersed to obtain graphene oxide dispersion. The concentration of high-acidity graphite oxide solution is 10-300 mg/mL. The concentration of graphene oxide is adjusted to 0.5-20 mg/mL, and encapsulated in synthetic organic polymer fabric bag. The resultant product is subjected to dialyzed cleaning process, and the pH is adjusted to 3 to obtain high-purity graphene oxide solution. The concentration of graphite oxide in the organic polymer synthetic fabric bag dilute solution is 0.5-20 mg/ml. The obtained graphene oxide solution is freeze-dried to obtain graphene oxide powder.