• 专利标题:   Preparation of composite material involves mixing copper sulfate pentahydrate, sulfuric acid, hydrochloric acid, graphene dispersion and water to form composite electrodeposition solution, electroplating, drying, pressing, and sintering.
  • 专利号:   CN111270097-A
  • 发明人:   TAO J, WANG M, YI J, LIU Y, BAO R, LI F, LI C, YOU X, TAN S
  • 专利权人:   UNIV KUNMING SCI TECHNOLOGY
  • 国际专利分类:   C22C001/10, C22C032/00, C22C009/00, C25D015/00, C25D003/58
  • 专利详细信息:   CN111270097-A 12 Jun 2020 C22C-001/10 202055 Pages: 7 Chinese
  • 申请详细信息:   CN111270097-A CN10221488 26 Mar 2020
  • 优先权号:   CN10221488

▎ 摘  要

NOVELTY - Preparation of composite material involves adding copper sulfate pentahydrate, sulfuric acid, hydrochloric acid and graphene dispersion to water, stirring thoroughly to mix evenly to obtain composite electrodeposition solution, pouring the composite electrodeposition solution into electroplating bath, placing two phosphorous copper plates as anode and titanium plate as cathode in the plating tank, connecting to direct current power supply, depositing having current density of 0.5-1.5 A.dm-2, preferably greater than or equal to 0.5 A.dm-2 for 5-10 hours, taking out the titanium plate, vacuum-drying, removing the composite film plated on the titanium plate, cutting the composite film material into desired shape, using two composite films deposited under different current densities to alternately stack, stacking to the required thickness, placing in hydraulic press for preloading, and sintering the pre-pressed material. USE - Preparation of composite material. ADVANTAGE - The method adopts composite electrodeposition method to ensure structural integrity and excellent dispersion of graphene in the matrix, and has excellent comprehensive mechanical properties by introducing layered structure of the composite material.