• 专利标题:   Preparing sulfur-nitrogen co-doped graphene-supported cobalt sulfide nickel catalytic material for catalytic precipitation of water electrolysis, involves dissolving metal cobalt source, nickel source and thiourea in solvent.
  • 专利号:   CN108411324-A
  • 发明人:   JIANG Z, DENG B
  • 专利权人:   UNIV SOUTH CHINA TECHNOLOGY
  • 国际专利分类:   C01G053/00, C25B001/04, C25B011/06
  • 专利详细信息:   CN108411324-A 17 Aug 2018 C25B-001/04 201864 Pages: 13 Chinese
  • 申请详细信息:   CN108411324-A CN10269322 29 Mar 2018
  • 优先权号:   CN10269322

▎ 摘  要

NOVELTY - Preparing a sulfur-nitrogen co-doped graphene-supported cobalt sulfide nickel catalytic material involves dissolving a metal cobalt source, a nickel source and thiourea in a solvent, mixing by ultrasonic stirring, then adding aqueous ammonia dropwise, stirring and mixing to obtain a uniform solution, adding graphene oxide to the homogeneous solution. After ultrasonic mixing, hydrothermal treatment, centrifugal washing, and freeze-drying are performed to obtain a graphene-supported cobalt sulfide nickel catalytic material. The graphene-supported cobalt sulfide nickel composite is calcined under a nitrogen atmosphere and graphene oxide is reduced to obtain a sulfur-nitrogen co-doped graphene-supported cobalt sulfide nickel catalyst material. USE - Method for preparing sulfur-nitrogen co-doped graphene-supported cobalt sulfide nickel catalytic material for catalytic precipitation of water electrolysis and oxygen evolution (claimed) and for water-cracking cathode and anode catalytic materials. ADVANTAGE - The method enables to prepare sulfur-nitrogen co-doped graphene-supported cobalt sulfide nickel catalytic material in simple manner with low cost, low energy consumption and is environmentally friendly, has good electrical conductivity and electrochemical catalytic properties.