• 专利标题:   Preparing graphene loaded iron-oxide self assembled mulberry structure lithium ion battery cathode material involves dispersing graphene oxide solid in alcohol to obtain solution, then using ultrasonic generator to uniformly disperse.
  • 专利号:   CN107452943-A
  • 发明人:   CAO L, MA M, QI H, LI J, HUANG J, WU G, CHEN W, YAO K
  • 专利权人:   UNIV SHAANXI SCI TECHNOLOGY
  • 国际专利分类:   H01M010/0525, H01M004/36, H01M004/52, H01M004/62
  • 专利详细信息:   CN107452943-A 08 Dec 2017 H01M-004/36 201803 Pages: 10 Chinese
  • 申请详细信息:   CN107452943-A CN10568025 13 Jul 2017
  • 优先权号:   CN10568025

▎ 摘  要

NOVELTY - Preparing graphene loaded iron-oxide self assembled mulberry structure lithium ion battery cathode material involves dispersing the graphene oxide solid in 25-45 mL alcohol to obtain solution of 1-5 milligram/mL, then using ultrasonic generator to form the uniformly dispersed graphene oxide suspension-A. The analysis-soluble iron salt ferrous chloride is added into 5-25 mL de-ionized water, stirred and fully dissolved, then added to suspension-A to prepare mixed solution-B, and added into iron salt and oxidized graphite alkene, where the concentration of the iron salt is 0.05-0.5 mole/L. USE - Method for preparing graphene loaded iron-oxide self assembled mulberry structure lithium ion battery cathode material (claimed). ADVANTAGE - The method enables to prepare graphene loaded iron-oxide self assembled mulberry structure lithium ion battery cathode material which is esay to process in a simple and cost-effective manner, easy to realize. It realizes the iron oxide in situ growth of graphene surface. DETAILED DESCRIPTION - Preparing graphene loaded iron-oxide self assembled mulberry structure lithium ion battery cathode material involves dispersing the graphene oxide solid in 25-45 mL alcohol to obtain solution of 1-5 milligram/mL, then using ultrasonic generator to form the uniformly dispersed graphene oxide suspension-A. The analysis-soluble iron salt ferrous chloride is added into 5-25 mL de-ionized water, stirred and fully dissolved, then added to suspension-A to prepare mixed solution-B, and added into iron salt and oxidized graphite alkene, where the concentration of the iron salt is 0.05-0.5 mole/L. The mixed solution-B is put into homogeneous hydro-thermal reaction kettle, then the reaction kettle is sealed, put into homogeneous hydrothermal reactor for hydrothermal reaction at 50-150 degrees C, and after finishing reaction, naturally cooled to room temperature to obtain product-C. The product-C is washed by water and alcohol and dispersed in water to obtain product-D. The product-D is frozen to be free of liquid, then put into freeze drier for drying at 10-50 Pascal for 10-20 hours to obtain the final graphene loaded iron oxide self-assembled mulberry structure lithium ion battery cathode material.