• 专利标题:   Chemical vapor deposition based preparation method of silicon doped graphene material used in e.g. optoelectronic technology field, involves heating treated substrate and carrying out reaction in presence of carbon source gas.
  • 专利号:   CN105463401-A
  • 发明人:   LIN S, LI X, XU W, ZHANG C
  • 专利权人:   UNIV ZHEJIANG
  • 国际专利分类:   C23C016/26
  • 专利详细信息:   CN105463401-A 06 Apr 2016 C23C-016/26 201648 Pages: 7 English
  • 申请详细信息:   CN105463401-A CN10872505 02 Dec 2015
  • 优先权号:   CN10872505

▎ 摘  要

NOVELTY - Chemical vapor deposition based preparation method of silicon doped graphene material, involves cleaning a substrate, carrying out argon plasma treatment, placing the treated substrate within a reactor, maintaining atmospheric pressure or vacuum within the reactor, introducing hydrogen at flow of 0.1-2000 sccm and at heating rate of 1-300 degrees C/minutes, then heating at 800-1800 degrees C, introducing carbon source gas and silicon source gas, carrying out reaction for 1-600 minutes, then carrying out quenching process at heating rate of 1-500 degrees C/minutes, and cooling to room temperature. USE - Chemical vapor deposition based preparation method of silicon doped graphene material used in optoelectronic technology and micro-nano device fabrication fields. ADVANTAGE - The problems of zero band gap graphene material are solved. DETAILED DESCRIPTION - Chemical vapor deposition based preparation method of silicon doped graphene material, involves cleaning a substrate, carrying out argon plasma treatment for 1-60 minutes at 10-500 watts, placing the treated substrate within a reactor, maintaining atmospheric pressure or vacuum within the reactor, introducing hydrogen at flow of 0.1-2000 sccm and at heating rate of 1-300 degrees C/minute, then heating at 800-1800 degrees C, introducing carbon source gas and silicon source gas in a flow rate ratio of 1:10-10000:1, carrying out reaction for 1-600 minutes, then carrying out quenching process at heating rate of 1-500 degrees C/minute, and cooling to room temperature.