• 专利标题:   Electrochemical preparation method of molybdenum disulfide/graphene composite electrode used for dye-sensitized solar cell, involves mixing graphene oxide/lithium perchlorate, and ammonium tetrathiomolybdate/potassium chloride.
  • 专利号:   CN105405663-A, CN105405663-B
  • 发明人:   LI S, MIN H, NI Y, SUN L, XU F, ZHU C
  • 专利权人:   UNIV SOUTHEAST
  • 国际专利分类:   H01G009/20
  • 专利详细信息:   CN105405663-A 16 Mar 2016 H01G-009/20 201635 Pages: 8 English
  • 申请详细信息:   CN105405663-A CN10729208 30 Oct 2015
  • 优先权号:   CN10729208

▎ 摘  要

NOVELTY - Electrochemical preparation method of molybdenum disulfide/graphene composite electrode involves mixing aqueous solution of graphene oxide/lithium perchlorate as electrolyte, electrically depositing graphene oxide films on fluorine-doped tin oxide (FTO) conductive glass, carrying out electrochemical reduction of graphene oxide film to obtain graphene film, using graphene film as substrate, mixing ammonium tetrathiomolybdate/potassium chloride aqueous solution to obtain molybdenum disulfide/graphene composite electrode. USE - Electrochemical preparation method of molybdenum disulfide/graphene composite electrode used for dye-sensitized solar cell. ADVANTAGE - The method enables the electrochemical preparation of molybdenum disulfide/graphene composite electrode without any post-treatment process. DETAILED DESCRIPTION - Electrochemical preparation method of molybdenum disulfide/graphene composite electrode involves providing electrochemical deposition system with three electrodes, mixing aqueous solution of graphene oxide/lithium perchlorate as electrolyte, electrically depositing graphene oxide films on fluorine-doped tin oxide (FTO) conductive glass, carrying out electrochemical reduction of graphene oxide film to obtain graphene film, using graphene film as substrate, mixing ammonium tetrathiomolybdate/potassium chloride aqueous solution to obtain molybdenum disulfide/graphene composite electrode.