• 专利标题:   Hydrothermal synthesis of metal oxide/graphene nanocomposite used in e.g. lithium battery, involves uniformly dispersing graphene oxide or partially reduced graphene in organic solvent of metal salt, dripping deionized water and stirring.
  • 专利号:   CN106099063-A, CN106099063-B
  • 发明人:   LI Y, ZHU Z, OU Z, HUANG Y, FU C, SU W, ZHANG H, ZHU J, OU C
  • 专利权人:   UNIV GUANGDONG TECHNOLOGY, UNIV GUANGDONG TECHNOLOGY
  • 国际专利分类:   B82Y030/00, H01G011/30, H01G011/36, H01G011/46, H01M010/0525, H01M004/36, H01M004/48, H01M004/52, H01M004/587, H01M004/62
  • 专利详细信息:   CN106099063-A 09 Nov 2016 H01M-004/36 201701 Pages: 9 Chinese
  • 申请详细信息:   CN106099063-A CN10607847 28 Jul 2016
  • 优先权号:   CN10607847

▎ 摘  要

NOVELTY - The hydrothermal synthesis of metal oxide/ graphene nanocomposite, involves (i) uniformly dispersing graphene oxide or partially reduced graphene in organic solvent of metal salt, dripping deionized water, stirring to obtain a homogeneous dispersion of graphene and metal salt, (ii) transferring the dispersion to a hydrothermal reaction kettle, performing hydrothermal reaction, cooling naturally, and obtaining hydrothermal product of metal oxide/graphene nanocomposite, (iii) suction-filtering, washing and drying to obtain metal oxide/graphene nanocomposite. USE - Hydrothermal synthesis of metal oxide/graphene nanocomposite used in lithium battery and supercapacitor (all claimed). ADVANTAGE - The metal oxide/ graphene nanocomposite is prepared by a simple method at low cost under low water temperature condition, while ensuring large-scale production safety. The metal oxide/ graphene nanocomposite achieves high specific capacity, super high rate performance and high cycle stability of the electrochemical properties. DETAILED DESCRIPTION - The hydrothermal synthesis of metal oxide/ graphene nanocomposite, involves (i) uniformly dispersing graphene oxide or partially reduced graphene in an organic solvent of metal salt, dripping deionized water, stirring for 5-120 minutes to obtain a homogeneous dispersion of graphene and metal salt, (ii) transferring the dispersion to a hydrothermal reaction kettle, and performing hydrothermal reaction at 80-120 degrees C for 0.1-72 hours, cooling naturally, and obtaining hydrothermal product of metal oxide/graphene nanocomposite, (iii) filtering the obtained product through suction, washing and drying to obtain metal oxide/graphene nanocomposite.