• 专利标题:   Preparation of titania/graphene-modified butyronitrile composite rubber, involves reducing titania/graphene oxide composite nanopowder, adding to butyronitrile emulsion, stirring, adding precipitator, shearing, washing, and drying.
  • 专利号:   CN112225964-A
  • 发明人:   LI J
  • 专利权人:   LINGSHA TRADE DONGGUAN CO LTD
  • 国际专利分类:   B82Y030/00, B82Y040/00, C01B032/198, C01G023/053, C08K003/04, C08K003/22, C08L009/04
  • 专利详细信息:   CN112225964-A 15 Jan 2021 C08L-009/04 202115 Pages: 8 Chinese
  • 申请详细信息:   CN112225964-A CN11107531 16 Oct 2020
  • 优先权号:   CN11107531

▎ 摘  要

NOVELTY - Preparation of titania/graphene-modified butyronitrile composite rubber, involves adding hydrochloric acid aqueous solution to a mixed solution of ethanol and benzyl alcohol, and stirring to obtain solution (A), adding titanium tetrachloride to a mixed solution of ethanol and benzyl alcohol, and stirring to obtain solution (B), simultaneously dripping solution (B) and graphene oxide solution in solution (A), stirring at high speed to obtain a titania/graphene oxide composite sol, adding the sol to a supercritical fluid device, extracting under the action of supercritical carbon dioxide fluid, drying to obtain a titania/graphene oxide composite nanopowder, vacuum heating and reducing the nanopowder to obtain a titania/graphene composite nanopowder, adding the nanopowder to a butyronitrile emulsion, stirring, adding a precipitator, shearing, washing, and drying. USE - Preparation of titania/graphene-modified butyronitrile composite rubber (claimed). DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for the titania/graphene modified butyronitrile composite rubber comprising titania/graphene composite nanopowder and butyronitrile emulsion in a mass ratio of 1:80-100.