• 专利标题:   Preparation of two-dimensional inorganic layered compound/graphene composite material for catalytic and electrochemical energy storage, involves mixing layered compound solution and graphene oxide solution, centrifuging, and washing.
  • 专利号:   CN104183830-A
  • 发明人:   LIU H, LIU W, HU Z
  • 专利权人:   UNIV CENT SOUTH
  • 国际专利分类:   H01G011/26, H01G011/32, H01G011/86, H01M004/139, H01M004/1393, H01M004/88, H01M004/96
  • 专利详细信息:   CN104183830-A 03 Dec 2014 H01M-004/1393 201511 Pages: 7 Chinese
  • 申请详细信息:   CN104183830-A CN10408483 19 Aug 2014
  • 优先权号:   CN10408483

▎ 摘  要

NOVELTY - Two-dimensional inorganic layered compound precursor is reduced into nanosheets using solvent with peeling energy, such that the layered compound is provided with positive charge, to obtain positively-charged layered compound solution. Obtained solution and negatively-charged graphene oxide solution are mixed, supernatant is decanted, centrifuged, and washed, to obtain two-dimensional inorganic layered compound/graphene composite material (A). Obtained composite material is reduced, to obtain two-dimensional inorganic layered compound/graphene composite material (B). USE - Preparation of two-dimensional inorganic layered compound/graphene composite material used for catalytic and electrochemical energy storage. ADVANTAGE - The two-dimensional inorganic layered compound/graphene composite material having excellent electroconductivity and stability, is manufactured. DETAILED DESCRIPTION - Two-dimensional inorganic layered compound precursor is reduced into nanosheets using solvent with peeling energy, such that the layered compound is provided with positive charge, to obtain positively-charged layered compound solution. The mass ratio of layered compound and solvent in positively-charged layered compound solution is 1:1-1:20. Positively-charged layered compound solution and negatively-charged graphene oxide solution are mixed, supernatant is decanted, centrifuged, and washed, to obtain two-dimensional inorganic layered compound/graphene composite material (A). Obtained composite material is reduced, to obtain two-dimensional inorganic layered compound/graphene composite material (B). The mass ratio of layered compound and solvent is 1:1-1:20.