• 专利标题:   Preparing graphene comprises adding hexabromobenzene and substance (copper bromide, copper iodide, copper chloride, copper or nickel) into solvent, stirring, heating under e.g. normal pressure in anaerobic environment or aerobic environment.
  • 专利号:   CN102320597-A, CN102320597-B
  • 发明人:   LIU H, QIN X, WANG L
  • 专利权人:   UNIV TIANJIN
  • 国际专利分类:   B82Y040/00, C01B031/04
  • 专利详细信息:   CN102320597-A 18 Jan 2012 C01B-031/04 201224 Pages: 8 Chinese
  • 申请详细信息:   CN102320597-A CN10198709 15 Jul 2011
  • 优先权号:   CN10198709

▎ 摘  要

NOVELTY - Preparing graphene comprises adding hexabromobenzene and substance A into a solvent, stirring, heating for 2-48 hours at 100-200 degrees C under normal pressure or pressurizing pressure in an anaerobic environment or aerobic environment. The ratio of hexabromobenzene, substance A and the solvent is (0.1-50 mg):(0.05-500 mg):(1 ml). The solvent is diethylene glycol dimethyl ether, diphenyl ether, ethyl ether, tetrahydrofuran, toluene or benzene. The substance A is copper bromide, copper iodide, copper chloride, copper or nickel. USE - The method is useful for preparing graphene. ADVANTAGE - The method has simple technique and requires moderate reaction condition.