• 专利标题:   Production of graphene supercapacitor electrode material for fast charge and discharge power applications, involves adding solvent, dripping aniline concentration to oxidized graphene dispersion, adding ammonium persulfate.
  • 专利号:   CN106710892-A
  • 发明人:   TAN Z, YAO Y, LIU Z
  • 专利权人:   UNIV DALIAN TECHNOLOGY
  • 国际专利分类:   C01B032/182, H01G011/36, H01G011/48, H01G011/86
  • 专利详细信息:   CN106710892-A 24 May 2017 H01G-011/36 201750 Pages: 10 Chinese
  • 申请详细信息:   CN106710892-A CN11159513 15 Dec 2016
  • 优先权号:   CN11159513

▎ 摘  要

NOVELTY - The method for producing graphene supercapacitor electrode material, involves preparing graphene oxide by Hummers method, adding solvent, dripping aniline concentration to oxidized graphene dispersion, ultrasonically dispersing evenly, adding acid to adjust pH of the solution to less than 2, adding concentration of ammonium persulfate, continuously stirring to obtain suspension, carrying out solvent thermal reduction, transferring the resulting suspension to reaction kettle, filtering the resulting product, washing and freeze-drying to obtain final product. USE - Method for producing graphene supercapacitor electrode material for fast charge and discharge power applications. ADVANTAGE - The environmentally-friendly method enables simple and efficient production of graphene supercapacitor electrode material with high specific capacitance, excellent magnification performance and high yield. DETAILED DESCRIPTION - Method for producing graphene supercapacitor electrode material, involves (1) preparing graphene oxide by Hummers method, adding solvent, (2) dripping 0.08-0.33 M concentration of aniline to 1.0-4.5 g/L concentration of oxidized graphene dispersion, ultrasonically dispersing evenly, (3) adding acid to adjust pH of the solution to less than 2, (4) adding 0.021-0.084 M concentration of ammonium persulfate, continuously stirring to obtain suspension, carrying out solvent thermal reduction, transferring the resulting suspension to reaction kettle at 100 degrees C for 5 hours, filtering the resulting product, washing and freeze-drying to obtain final product.