• 专利标题:   Preparing graphene ultra-violet curing adhesive comprises mixing ultra-violet resin and graphene, stirring, dispersing, adding surfactant and leveling agent, mixing, heating, cooling, heating and mixing.
  • 专利号:   CN107090252-A
  • 发明人:   HOU S, ZHANG R, SHEN H
  • 专利权人:   WUXI YUNTING GRAPHENE TECHNOLOGY CO LTD
  • 国际专利分类:   B32B037/12, B32B038/00, C03C027/12, C09J011/04, C09J011/06, C09J011/08, C09J163/00, C09J167/00, C09J171/00, C09J175/04, C09J183/04, C09J004/02, C09J004/06
  • 专利详细信息:   CN107090252-A 25 Aug 2017 C09J-004/06 201766 Pages: 12 Chinese
  • 申请详细信息:   CN107090252-A CN10256665 19 Apr 2017
  • 优先权号:   CN10256665

▎ 摘  要

NOVELTY - Preparing graphene ultra-violet curing adhesive comprises (i) mixing ultra-violet resin B and graphene, stirring at 40-50 degrees C and dispersing for 1-3 hours; (ii) adding surfactant and leveling agent, mixing uniformly at 20-30 degrees C, pouring the ultrasonic dispersed mixture at 40-50 degrees C, heating at 20-30 degrees C, mixing at 600-1000 revolutions/minutes for 5-15 minutes and cooling to 10-20 degrees C; and (iii) heating to 20-30 degrees C, stirring at 1100-1500 revolutions/minutes for 10-30 minutes, heating at 10-20 degrees C for 1-3 hours, mixing at 100-400 revolutions/minutes. USE - The method is useful for preparing graphene ultra-violet curing adhesive (claimed). ADVANTAGE - The adhesive has fast drying speed and is environmentally-friendly and suitable for industrial production. DETAILED DESCRIPTION - Preparing graphene ultra-violet curing adhesive comprises (i) mixing ultra-violet resin B and graphene, stirring at 40-50 degrees C and dispersing for 1-3 hours; (ii) adding surfactant and leveling agent, mixing uniformly at 20-30 degrees C, pouring the ultrasonic dispersed mixture at 40-50 degrees C, heating at 20-30 degrees C, mixing at 600-1000 revolutions/minutes for 5-15 minutes and cooling to 10-20 degrees C; and (iii) heating to 20-30 degrees C, stirring at 1100-1500 revolutions/minutes for 10-30 minutes, heating at 10-20 degrees C for 1-3 hours, mixing at 100-400 revolutions/minutes, where the mass ratio of the ultra violet resin B, graphene, surfactant and leveling agent is 1:1-5:0.1-0.5:1-5.