• 专利标题:   Preparing high-dispersive magnetic separation and reduction graphene oxide/iron oxide/nano silver grade structure material comprises e.g. mixing ferrous salt aqueous solution and graphene oxide water dispersion mixture, and drying.
  • 专利号:   CN106964365-A, CN106964365-B
  • 发明人:   ZHAO S, JIANG H, LU C, CHAO T, GAO Q, ZHANG Z
  • 专利权人:   UNIV JINAN
  • 国际专利分类:   B01J023/89, B01J037/04
  • 专利详细信息:   CN106964365-A 21 Jul 2017 B01J-023/89 201756 Pages: 8 Chinese
  • 申请详细信息:   CN106964365-A CN10203188 30 Mar 2017
  • 优先权号:   CN10203188

▎ 摘  要

NOVELTY - Preparing high-dispersive magnetic separation and reduction graphene oxide/iron oxide/nano silver grade structure material comprises e.g. (i) mixing ferrous salt aqueous solution and graphene oxide water dispersion mixture, stirring, adding aqueous ammonia to form first solution, (ii) dissolving silver nitrate in deionized water to form silver nitrate solution, adding aqueous ammonia to obtain silver ammonia solution, and adding into first solution, mixing and reacting, cooling reaction system to room temperature, filtering, and washing residue with deionized water, and drying in vacuum. USE - The highly dispersive magnetic separation and reduction graphene oxide/iron oxide/nano silver grade structured material is useful in the field of organic dye reduction and degradation (claimed). ADVANTAGE - The layered structure material solves intermolecular stacking of graphene sheets, and has excellent performance including high dispersibility, high catalytic activity and magnetic field assisted separation; and preparation method has mild reaction condition, and is suitable for large-scale industrial production. DETAILED DESCRIPTION - Preparing high-dispersive magnetic separation and reduction graphene oxide/iron oxide/nano silver grade structure material comprises (i) mixing ferrous salt aqueous solution and graphene oxide water dispersion mixture, stirring, adding aqueous ammonia, adjusting system pH to 7-14 to form first solution, (ii) dissolving silver nitrate in deionized water to form silver nitrate solution, adding aqueous ammonia to obtain silver ammonia solution, and then adding into first solution, mixing and reacting at 60-100 degrees C for 3-12 hours, cooling reaction system to room temperature, filtering, and washing residue with deionized water, and drying in vacuum.