• 专利标题:   Preparation of graphene involves stirring natural graphite powder and acid, removing excess acid, adding additive, injecting obtained low-temperature graphite slurry into reactor filled with supercritical fluid medium, and filtering.
  • 专利号:   CN104229787-A, CN104229787-B
  • 发明人:   LIU C, HU G, GAO H
  • 专利权人:   UNIV SHANGHAI JIAOTONG
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN104229787-A 24 Dec 2014 C01B-031/04 201518 Pages: 7 Chinese
  • 申请详细信息:   CN104229787-A CN10478317 18 Sep 2014
  • 优先权号:   CN10478317

▎ 摘  要

NOVELTY - Natural graphite powder and acid are added into a container, stirred, filtered, excess acid is removed, additive is added to the resultant product, and stirred. The resultant mixed material is transferred to a low-temperature container, and cooled, to obtain low-temperature graphite slurry. The obtained graphite slurry is quickly injected into a reactor filled with supercritical fluid medium, temperature and pressure of material in the reactor are controlled, processed, filtered, separated, and dried, to obtain graphene product. USE - Preparation of graphene (claimed). ADVANTAGE - The method enables preparation of graphene having excellent electrical and thermal properties with improved yield by approximately 2-5 times.