• 专利标题:   Preparation of manganese dioxide/graphene composite mesoporous nanospheres, involves dispersing graphene encapsulated by inert nano-oxide in mixed aqueous solution containing cetyltrimethylammonium bromide, ultrasonically reacting, hydrothermally reacting, washing, and drying.
  • 专利号:   CN113816366-A, CN113816366-B
  • 发明人:   MA X, YANG J, ZHANG J, LI J, TANG X, LI L, ZHOU X, DING Y, LUO W, TENG Y, XIE G
  • 专利权人:   UNIV CHONGQING POSTS TELECOM
  • 国际专利分类:   C01B032/194, C01G045/02, C09D163/00, C09D005/08
  • 专利详细信息:   CN113816366-A 21 Dec 2021 C01B-032/194 202242 Chinese
  • 申请详细信息:   CN113816366-A CN11333500 11 Nov 2021
  • 优先权号:   CN11333500

▎ 摘  要

NOVELTY - The preparation of manganese dioxide/graphene composite mesoporous nanospheres, involves dispersing graphene encapsulated by inert nano-oxide in mixed aqueous solution containing cetyltrimethylammonium bromide and sodium hydroxide, ultrasonically reacting, adding manganese tetrahydrate, dripping sodium hydroxide solution to adjust pH value to 10-11, hydrothermally reacting, cooling, adding reducing agent ethylene glycol to react, and centrifugally washing the product with absolute ethanol and deionized water, and drying. USE - Preparation of manganese dioxide/graphene composite mesoporous nanospheres (claimed). ADVANTAGE - The method enables preparing manganese dioxide/graphene composite mesoporous nanospheres by simple and easy process, the manganese oxide nanoparticles are uniformly dispersed on reduced graphene oxide, the average particle size of mesoporous nanospheres is about 500-800 nm, and the anticorrosive performance of the epoxy coating is improved. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for composite mesoporous nanosphere, which includes manganese dioxide nanoparticles dispersed on graphene encapsulated by inert nano oxide, where the particle size is 500-800 nm.