• 专利标题:   Preparing graphite alkene, comprises taking graphite powder, concentrated sulfuric acid, potassium permanganate powder, hydrogen peroxide, concentrated hydrochloric acid and deionized water as raw material to prepare acidic multi-impurity.
  • 专利号:   CN115231559-A
  • 发明人:   YANG D, SONG W, LV S, WU P
  • 专利权人:   CHANGSHU SUNMUN CHEM TECHNOLOGY CO LTD
  • 国际专利分类:   C01B032/184, C01B032/194
  • 专利详细信息:   CN115231559-A 25 Oct 2022 C01B-032/184 202307 Chinese
  • 申请详细信息:   CN115231559-A CN11018971 24 Aug 2022
  • 优先权号:   CN11018971

▎ 摘  要

NOVELTY - Method for preparing graphite alkene, involves (a) taking graphite powder, concentrated sulfuric acid, potassium permanganate powder, hydrogen peroxide, concentrated hydrochloric acid and deionized water as raw materials to prepare acidic multi-impurity graphene dispersion, then adding alkaline solution to adjust pH value, (b) adding carbonate or bicarbonate to multi-imperfection dispersion liquid obtained in step (a), stirring and reacting to obtain a multi-amino-dispersion graphene, (c) decompressing, distilling and concentrating graphene obtained adding non-aqueous solvent to crystal not increased, and stopping adding non-queous solvent, and (d) layering, filtering, water washing, drying and removing crystal in mixed solution. USE - Method is for preparing graphene, which is used in textile, coating, energy storage and conversion device. ADVANTAGE - Method is combined with redox process, alkali reduction process and waste water solvent crystallization stripping process to obtain less defect and high graphene. The graphene stability of water-based dispersion prepared by mixing graphene and surfactant is good, which can improve compatibility of dispersion in application system. DETAILED DESCRIPTION - INDEPENDENT CLAIMS are included for: (1) kind of graphene; (2) water-based graphene.