• 专利标题:   Preparation of polyacrylic acid-graphene oxide composite involves adding acrylic acid to graphene oxide dispersion, adding N,N-methylenebisacrylamide, heating mixture, and adding ammonium persulfate.
  • 专利号:   CN104530293-A
  • 发明人:   ZHANG M
  • 专利权人:   QINGDAO BAIZHONG CHEM TECHNOLOGY CO LTD
  • 国际专利分类:   C08F002/44, C08F220/06, C08F222/38, C08K003/04
  • 专利详细信息:   CN104530293-A 22 Apr 2015 C08F-220/06 201546 Pages: 4 Chinese
  • 申请详细信息:   CN104530293-A CN10754101 11 Dec 2014
  • 优先权号:   CN10754101

▎ 摘  要

NOVELTY - 5-10 pts. wt. Acrylic acid is added to 20-50 pts. wt. graphene oxide dispersion and rapidly-stirred. 16-20 pts. wt. N,N-methylenebisacrylamide is added to solution and rapidly-stirred, and nitrogen is supplied for 20-40 minutes and gas-substituted. After completion of gas replacement, the mixture is heated and 0.05-0.2 pts. wt. ammonium persulfate is quickly added to reaction system and heated. The reaction mixture is cooled to room temperature, washed with distilled water to neutral, dried, ground and sieved to 400-500 mesh, to obtain polyacrylic acid-graphene oxide composite. USE - Preparation of polyacrylic acid-graphene oxide composite (claimed). ADVANTAGE - The method enables preparation of polyacrylic acid-graphene oxide composite having excellent compatibility, water-absorbing property and salt resistance. DETAILED DESCRIPTION - 5-10 pts. wt. Acrylic acid is added to 20-50 pts. wt. graphene oxide dispersion and rapidly-stirred. 16-20 pts. wt. N,N-methylenebisacrylamide is added to solution at room temperature and rapidly-stirred, and nitrogen is supplied for 20-40 minutes and gas-substituted. After completion of gas replacement, the mixture is heated at 50-55 degrees C and 0.05-0.2 pts. wt. ammonium persulfate is quickly added to reaction system and heated at 70 degrees C for 3-5 hours. The reaction mixture is cooled to room temperature, washed with distilled water to neutral, dried at 60-80 degrees C for 24 hours, ground and sieved to 400-500 mesh, to obtain polyacrylic acid-graphene oxide composite.