• 专利标题:   Preparation of conductive anti-corrosion coating layer involves polishing magnesium alloy, performing micro-arc oxidation treatment, coating conductive anti-corrosion coating prepared using e.g. polypyrrole conductive material and epoxy resin, on surface of micro-arc oxidation layer, and drying.
  • 专利号:   CN114887858-A
  • 发明人:   LIU M, CHANG L, ZHU S, WANG L, GUAN S
  • 专利权人:   UNIV ZHENGZHOU
  • 国际专利分类:   B05D003/10, B05D005/00, B05D005/12, B05D007/14, B05D007/24, C25D011/30
  • 专利详细信息:   CN114887858-A 12 Aug 2022 B05D-005/12 202286 Chinese
  • 申请详细信息:   CN114887858-A CN10506015 11 May 2022
  • 优先权号:   CN10506015

▎ 摘  要

NOVELTY - Preparation of conductive anti-corrosion coating layer on surface of magnesium alloy micro-arc oxidation layer, involves polishing AZ91 magnesium alloy to obtain bright surface, performing micro-arc oxidation treatment on the magnesium alloy using micro-arc oxidation electrolyte, adding pyrrole monomer and sodium benzenesulfonate to deionized water or graphene suspension, adding an oxidant solution to obtain polypyrrole conductive material (A) or polypyrrole/graphene conductive composite material (B), dissolving 1-2 pts. wt. material (A or B), 10-15 pts. wt. epoxy resin and 4-6 pts. wt. polyamide curing agent in 6-10 pts. wt. n-butanol, spin-coating obtained conductive anti-corrosion coating on the surface of the micro-arc oxidation layer, and drying. The oxidant is ferric chloride. The molar ratio of pyrrole monomer, sodium benzenesulfonate and ferric chloride is 1-1.5:0.5-0.75:2-2.5. The usage amount of graphene is 10-20 wt.% with respect to pyrrole. USE - Preparation of conductive anti-corrosion coating layer (claimed) on surface of magnesium alloy micro-arc oxidation layer. The magnesium alloy is used in vehicle, aerospace, biological application and electronic product. ADVANTAGE - The method is simple and low cost. The coating obtained by the method has a certain conductive ability and a certain corrosion resistance.