• 专利标题:   Three-dimensional network structure reduced graphene oxide/cobalt oxide-iron oxide composite material is first connected by the cobalt oxide nanowire interconnecting reduced graphene oxide thin plates.
  • 专利号:   CN111584245-A
  • 发明人:   WANG Y, YANG H, CHEN Z, YU C, LI L, LU J, WEI H
  • 专利权人:   UNIV CHINA ELECTRONIC SCI TECHNOLOGY
  • 国际专利分类:   B82Y030/00, B82Y040/00, H01G011/24, H01G011/26, H01G011/36, H01G011/46, H01G011/86
  • 专利详细信息:   CN111584245-A 25 Aug 2020 H01G-011/24 202077 Pages: 10 Chinese
  • 申请详细信息:   CN111584245-A CN10373468 06 May 2020
  • 优先权号:   CN10373468

▎ 摘  要

NOVELTY - Three-dimensional network structure reduced graphene oxide/cobalt oxide-iron oxide composite material is first connected by the cobalt oxide nanowire interconnecting reduced graphene oxide thin plates to form a networked reduced graphene oxide/cobalt oxide, and then embedding iron oxide nanospheres to generate desired product. USE - Three-dimensional network structure reduced graphene oxide/cobalt oxide-iron oxide composite material. ADVANTAGE - The three-dimensional network structure reduced graphene oxide/cobalt oxide-iron oxide composite material improves the electrochemical performance of the composite material. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for a method for preparing three-dimensional network structure reduced graphene oxide/cobalt oxide-iron oxide composite material, which involves: (A) pouring the peeled graphene oxide into the reaction kettle; (B) using thermal reduction method to react for 8-48 h under the condition of 100-400 degrees C to obtain the concentration of 0.5-3mg/ml reduced graphene oxide/aqueous solution; (C) dispersing the cobalt salt aqueous solution and the mixed solution of urea and ammonium fluoride dissolved in ethanol in the reduced graphene oxide/aqueous solution; (D) transferring the mixture to the autoclave for 10-14 hours at a temperature of 180-220 degrees C; (E) neutralizing and stirring vigorously to dissolve; (F) adding ethanol dropwise; (G) transferring to an autoclave for reaction at a temperature of 180-220 degrees C for 22-26h; (H) carrying out centrifugal separation; (I) washing multiple times; and (J) drying to obtain desired product.