• 专利标题:   Preparing sheet-shaped half-metal molybdenum (IV) telluride:copper, and molybdenum (IV) telluride:copper/reduced graphene oxide comprises e.g. adding tellurium powder, and potassium borohydride to deionized water, reacting, and dissolving.
  • 专利号:   CN110560095-A
  • 发明人:   HE H, HE Z, SHEN Q
  • 专利权人:   UNIV SHAANXI SCI TECHNOLOGY
  • 国际专利分类:   B01J027/057, B01J037/10, C25B001/04, C25B011/06
  • 专利详细信息:   CN110560095-A 13 Dec 2019 B01J-027/057 201999 Pages: 10 Chinese
  • 申请详细信息:   CN110560095-A CN10935641 29 Sep 2019
  • 优先权号:   CN10935641

▎ 摘  要

NOVELTY - Preparing sheet-shaped half-metal molybdenum (IV) telluride:copper (MoTe2:Cu), and molybdenum (IV) telluride:copper/reduced graphene oxide (MoTe2:Cu/RGO) comprises (i) adding 0.002-0.004 mol tellurium powder, and 0.004-0.008 mol potassium borohydride to 10 ml deionized water, placing in a sealed environment, and reacting to obtain tellurium(II) ion precursor aqueous solution, (ii) dissolving 0.001/7x 0.965-0.002/7x 0.965 mol ammonium paramolybdate, and 0.000005-0.00001 mol copper acetate in 10 ml solvent, and then adding 0.0025-0.005 mol citric acid to obtain molybdenum ion source precursor solution, (iii) placing tellurium(II) ion precursor aqueous solution, and molybdenum ion source precursor solution in a reaction kettle, maintaining at room temperature, then increasing the temperature to 155-165 degrees C, performing hydrothermal reaction, cooling to room temperature, filtering, washing the filtrate, and drying to obtain the finished product. USE - The method is useful for preparing sheet-shaped half-metal molybdenum (IV) telluride:copper, and molybdenum (IV) telluride:copper/reduced graphene oxide. ADVANTAGE - The method: directly produces metal molybdenum telluride with a semi-metal structure; and is simple to process.