• 专利标题:   Preparation of graphene solution for forming e.g. photoelectric functional material, involves reacting dispersion containing graphite and polyvinylpyrrolidone in supercritical carbon dioxide reaction apparatus.
  • 专利号:   CN104130538-A, CN104130538-B
  • 发明人:   XU S, WANG N, XU Q, ZHAO Y
  • 专利权人:   UNIV ZHENGZHOU
  • 国际专利分类:   C01B031/04, C08K003/04, C08L039/06
  • 专利详细信息:   CN104130538-A 05 Nov 2014 C08L-039/06 201504 Pages: 7 Chinese
  • 申请详细信息:   CN104130538-A CN10332764 14 Jul 2014
  • 优先权号:   CN10332764

▎ 摘  要

NOVELTY - Preparation of graphene solution involves dispersing 25-50 mg graphite and 100-200 mg polyvinylpyrrolidone in 5-10 ml water or ethanol, placing resultant dispersion in supercritical carbon dioxide reaction apparatus, reacting at 40-45 degrees C and 6-20 MPa for 0.5-7 hours under stirring condition, and lowering pressure to atmospheric pressure. USE - Preparation of graphene solution used for graphene composite material, photoelectric functional material and biomedical applications. ADVANTAGE - The method enables preparation of graphene solution having high quality and suppressed defect, with high yield, by simple, environmentally-friendly and economical process.