• 专利标题:   Thermoplastic glucomannan/graphene oxide composite material used in chemical industry, comprises specific amount of thermoplastic glucomannan, oxidized graphene, crosslinking agent and plasticizer.
  • 专利号:   CN102675804-A, CN102675804-B
  • 发明人:   DUAN T, LUO X, WU F, ZHU W, ZHANG L
  • 专利权人:   UNIV SOUTHWEST SCI TECHNOLOGY
  • 国际专利分类:   C08B037/00, C08F251/00, C08K003/04, C08K009/00, C08L051/02
  • 专利详细信息:   CN102675804-A 19 Sep 2012 C08L-051/02 201318 Pages: 12 Chinese
  • 申请详细信息:   CN102675804-A CN10153668 17 May 2012
  • 优先权号:   CN10153668

▎ 摘  要

NOVELTY - A thermoplastic glucomannan/graphene oxide composite material comprises (in parts weight) thermoplastic glucomannan (1-99), oxidized graphene (0.00l-2), crosslinking agent (0-10) and plasticizer (0-10). USE - Thermoplastic glucomannan/graphene oxide composite material is used in chemical industry, medical field and airport construction. ADVANTAGE - The thermoplastic glucomannan/graphene oxide composite material has excellent performance, adsorptivity, thermal stability and mechanical toughness, and is biodegradable and environmentally-friendly, and can be regenerated. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for preparation of thermoplastic glucomannan/graphene oxide composite material. Thermoplastic glucomannan (in parts weight) (1-99), oxidized graphene (0.00l-2), crosslinking agent (0-10) and plasticizer (0-10)are mixed and dried. The resulted mixture is added into ethanol or aqueous solution of graphene oxide, mechanically stirred for 5-10 hours, to mix uniformly, filtered, the solid is dried at 80-110 degrees C for 1-3 hours, obtain dried mixture. Ethanol or aqueous solution of graphene oxide (0.01-20 g/L) is prepared by dissolving graphene oxide in ethanol or water and modifying by ultrasonic treatment for 1-5 inches for 300-1000 W in ultrasonic device. The dried mixture is blended with crosslinking agent and plasticizer, stirred uniformly in a mixer at 20-60 degrees C for 5-30 minutes, dried for 8-12 hours, to blend the dried mixture. The blend is put into a double screw extruder, extruded at 100-140 degrees C for 5-15 hours at 0.1-1 MPa and palletized, to obtain thermoplastic glucomannan/graphene oxide composite material.