• 专利标题:   Preparation of graphene three-dimensional porous structure powder involves adding catalyst metal salt with water, mixing with polymer, stirring, filtering, taking the residue, cleaning, drying, adding reducing agent solution and stirring.
  • 专利号:   CN106744859-A
  • 发明人:   SHEN P, SHI W, TIAN Z, ZHANG Y, ZHU J
  • 专利权人:   UNIV GUANGXI
  • 国际专利分类:   C01B032/184
  • 专利详细信息:   CN106744859-A 31 May 2017 C01B-032/184 201754 Pages: 13 Chinese
  • 申请详细信息:   CN106744859-A CN10053883 22 Jan 2017
  • 优先权号:   CN10053883

▎ 摘  要

NOVELTY - Preparation of graphene three-dimensional porous structure powder comprises adding catalyst metal salt with water to obtain 10-60% metal salt solution, mixing with polymer, stirring for 0.1-12 hours, filtering, taking the residue, cleaning, drying, adding reducing agent solution, stirring for 0.1-12 hours, filtering, taking filter residue, drying, adding pore-forming agent with relative ratio of 0.2-2, stirring, drying, heating in a protective atmosphere at 700-1000 degrees C for 0.5-8 hours, adding to acidic solution, pickling for 1-12 hours, filtering and drying. USE - Method for preparing graphene three-dimensional porous structure powder (claimed). ADVANTAGE - The product has high specific surface area and high conductivity. The method is short and has high yield and reduced cost.