• 专利标题:   Milling white graphene comprises mixing white graphene powder, surfactant and ball milling medium, dissolving, ball milling, washing the resulting powder with alcohol and drying.
  • 专利号:   CN106744875-A, WO2018107795-A1
  • 发明人:   DUAN X, JIANG H, WANG J
  • 专利权人:   GUANGDONG NALU NANOTECHNOLOGY CO LTD, GUANGDONG NANOLUTION SCI TECHNOLOGY CO
  • 国际专利分类:   C01B032/19, C01B021/064
  • 专利详细信息:   CN106744875-A 31 May 2017 C01B-032/19 201750 Pages: 8 Chinese
  • 申请详细信息:   CN106744875-A CN11140745 12 Dec 2016
  • 优先权号:   CN11140745

▎ 摘  要

NOVELTY - Milling white graphene comprises mixing the white graphene powder, surfactant and ball milling medium, dissolving, ball milling in a sealed ball mill, adding the ball milling media after each period of milling, where the addition of the ball mill medium is 5-40 wt.% of the white graphene and milling for 120-480 hours, washing the resulting powder with alcohol and drying. USE - The method is useful for milling white graphene (claimed). ADVANTAGE - The method: can effectively peel off white graphene particles; produces white graphene with uniform particles, few layers and large area and high purity; and can be dispersed in alcohol and other solvents to save dozens of days to not produce agglomeration settlement. DETAILED DESCRIPTION - Milling white graphene comprises (a) mixing the white graphene powder, surfactant and ball milling medium, dissolving, ball milling at a rate of 200-800 revolutions/minute in a sealed ball mill, where the mass ratio of the white graphene powder and the surfactant is 1:1-500:1 and the mass ratio of the white graphene and the ball milling medium is 2:1-1:10, (b) adding the ball milling media after each period of milling, where the addition of the ball mill medium is 5-40 wt.% of the white graphene and milling for 120-480 hours and (c) washing the resulting powder with alcohol and drying, to obtain white ball graphene dispersion.