• 专利标题:   Processing salt-containing wastewater based on microelectrolysis by preparing graphene oxide dispersion liquid, atomizing and granulating, directly curing particles by liquid nitrogen, freeze drying, and placing in iron salt solution.
  • 专利号:   CN112408553-A, CN112408553-B
  • 发明人:   XIE W, GU L, CHEN S, LU X, CHEN J
  • 专利权人:   ZHEJIANG XIESHI NEW MATERIALS CO LTD
  • 国际专利分类:   C02F001/461
  • 专利详细信息:   CN112408553-A 26 Feb 2021 C02F-001/461 202130 Pages: 7 Chinese
  • 申请详细信息:   CN112408553-A CN11194735 30 Oct 2020
  • 优先权号:   CN11194735

▎ 摘  要

NOVELTY - Processing salt-containing wastewater based on microelectrolysis includes preparing graphene oxide dispersion liquid, atomizing and granulating the graphene oxide dispersion liquid by spraying, directly curing the particles after granulation by liquid nitrogen, and freeze drying to obtain porous graphene oxide gel microsphere; placing the porous graphene oxide gel microsphere in iron salt solution, stirring and mixing, dropping sodium borohydride solution, rapidly stirring, and drying the solid obtained by reaction to obtain graphene porous gel loaded nano-zero-valent iron material; uniformly mixing the prepared graphene porous gel loaded nano-zero-valent iron material, carbon powder, urea, clay, and deionized water, and granulating, and sintering to obtain porous microelectrolysis filler; and putting the prepared porous microelectrolysis filler in a reactor. USE - The method is for processing salt-containing wastewater based on microelectrolysis. ADVANTAGE - The filler has rich pore structure, large specific surface area, and good adsorption performance, which can effectively improve the micro-electrolysis efficiency, so as to improve the treatment efficiency of the salt-containing wastewater. DETAILED DESCRIPTION - Processing salt-containing wastewater based on microelectrolysis comprises preparing graphene oxide dispersion liquid, atomizing and granulating the graphene oxide dispersion liquid by spraying, directly curing the particles after granulation by liquid nitrogen, and freeze drying to obtain porous graphene oxide gel microsphere; placing the porous graphene oxide gel microsphere in iron salt solution, stirring and mixing, dropping sodium borohydride solution, rapidly stirring, and drying the solid obtained by reaction to obtain graphene porous gel loaded nano-zero-valent iron material; uniformly mixing the prepared graphene porous gel loaded nano-zero-valent iron material, carbon powder, urea, clay, and deionized water, and granulating, and sintering to obtain porous microelectrolysis filler; and putting the prepared porous microelectrolysis filler in a reactor, continuously introducing salt-containing wastewater into the reactor, processing under stirring condition, and discharging the processed wastewater to industrial discharge standard.