• 专利标题:   Synthesizing graphene by using hydrothermal reaction, comprises e.g. dispersing montmorillonite and glucose in mixture of water and ethanol, placing homogeneous mixture in autoclave and heating, drying the resulting material and annealing.
  • 专利号:   PL411051-A1, PL225800-B1
  • 发明人:   CHEN X, MIJOWSKA E, KALENCZUK R, SKUMIAL P, SPERA P, MIJOWSKA S
  • 专利权人:   UNIV ZACHODNIOPOMORSKI TECHNOLOGICZNY, SKUMIAL P, SPERA P, MIJOWSKA S, SKUMIAL P, SPERA P
  • 国际专利分类:   C01B031/02
  • 专利详细信息:   PL411051-A1 01 Aug 2016 C01B-031/02 201661 Pages: 1
  • 申请详细信息:   PL411051-A1 PL411051 27 Jan 2015
  • 优先权号:   PL411051

▎ 摘  要

NOVELTY - Synthesizing graphene by using hydrothermal reaction, comprises: e.g. dispersing montmorillonite and glucose in a weight ratio of 1:1 plus minus 0.1 in a mixture of water and ethanol in a volume ratio of 2:1; placing the homogeneous mixture in an autoclave and heating to a temperature of 180-200 degrees C for 12-48 hours; and drying the resulting material at a temperature of 100 degrees C and then annealing in a furnace under an inert atmosphere for 4-6 hours. USE - The process is useful for synthesizing graphene by using hydrothermal reaction. DETAILED DESCRIPTION - Synthesizing graphene by using hydrothermal reaction, comprises: dispersing montmorillonite and glucose in a weight ratio of 1:1 plus minus 0.1 in a mixture of water and ethanol in a volume ratio of 2:1; placing the homogeneous mixture in an autoclave and heating to a temperature of 180-200 degrees C for 12-48 hours; drying the resulting material at a temperature of 100 degrees C and then annealing in a furnace under an inert atmosphere for 4-6 hours; removing the montmorillonite using concentrated solutions of sodium hydroxide or hydrofluoric acid, and further purifying the obtained flakes of graphene with concentrated hydrochloric acid; and curing the material in an oven at a temperature of 800-1000 degrees C, using an inert gas, argon or nitrogen. The step of removing montmorillonite and purification of flakes of graphene are carried out by long-term dispersion of the flakes of graphene and subsequent separation by filtration or centrifugation.