• 专利标题:   Method for preparing graphene, involves uniformly mixing layered compound and solvent, adding catalyst, adding aqueous solution of carbon source and catalyst-modified layered compound, introducing argon and adding nitric acid.
  • 专利号:   CN106241789-A, CN106241789-B
  • 发明人:   LU Y, SU Q, WANG J, ZHONG Z
  • 专利权人:   GUILIN XINYI REFRIGERATION EQUIP CO LTD, ZHONG Z
  • 国际专利分类:   C01B031/04, C01B032/184
  • 专利详细信息:   CN106241789-A 21 Dec 2016 C01B-031/04 201718 Pages: 7 Chinese
  • 申请详细信息:   CN106241789-A CN10747243 28 Aug 2016
  • 优先权号:   CN10747243

▎ 摘  要

NOVELTY - The method for preparing graphene, involves uniformly mixing layered compound and solvent, drying to obtain modified layered compound, adding catalyst, microwave processing to obtain catalyst-modified layered compound, adding aqueous solution of carbon source and catalyst-modified layered compound to obtain catalyst-modified layered compound suspension, filtering, transferring filtered mixture to reactor, introducing argon, naturally cooling to room temperature, adding nitric acid to remove layered compounds and filtering to obtain graphene. USE - Method for preparing graphene (claimed). ADVANTAGE - The method enables simple preparation of graphene with low production cost and protected structure. DETAILED DESCRIPTION - Method for preparing graphene involves uniformly mixing layered compound and solvent, ultrasonically processing at 50-70 degrees C for 30-60 minutes, washing, drying to obtain modified layered compound, adding catalyst, microwave processing at rated power of 500-600 W for 10-20 minutes to obtain catalyst-modified layered compound, adding aqueous solution of carbon source and catalyst-modified layered compound to obtain catalyst-modified layered compound suspension, ultrasonically processing or mechanical stirring at vacuum pressure of 5-20 MPa, filtering, transferring the filtered mixture to high-temperature reactor, introducing argon at the rate of 80-100 mL/minute, controlling the reactor temperature at 800-1000 degrees C for 3-8 hours, naturally cooling to room temperature, adding 30-50 wt.% nitric acid to remove layered compounds and filtering to obtain graphene.