• 专利标题:   Preparing metal sulfide/graphene for sodium ion battery, involves adding graphene oxide in ionic liquid, ultrasonically dispersing to obtain graphene oxide dispersion, adding metal source to graphene oxide dispersion and dispersing.
  • 专利号:   CN107017392-A
  • 发明人:   YAN Y, PAN Z, CUI N, XIE J, MOU W, HAO X, LIU L, LI Z
  • 专利权人:   UNIV DALIAN TECHNOLOGY
  • 国际专利分类:   H01M010/054, H01M004/36, H01M004/58, H01M004/62
  • 专利详细信息:   CN107017392-A 04 Aug 2017 H01M-004/36 201760 Pages: 7 Chinese
  • 申请详细信息:   CN107017392-A CN10305997 04 May 2017
  • 优先权号:   CN10305997

▎ 摘  要

NOVELTY - Preparing metal sulfide/graphene involves adding graphene oxide in the ionic liquid, ultrasonically dispersing to obtain graphene oxide dispersion, adding the metal source to the graphene oxide dispersion, continuously ultrasonically dispersing to obtain the precursor. The sulfur source is added into the precursor to react at 150-220 degrees C for 8-20 hours, then the obtained product is washed, dried and calcined in tubular furnace in protection of inert atmosphere at 350-550 degrees C for 3-6 hours to obtain the metal sulfide/graphene. USE - Method for preparing metal sulfide/graphene for sodium ion battery (claimed). ADVANTAGE - The method enables to prepare metal sulfide/graphene which is easy to process in a simple and cost-effective manner. It has high conductivity, good structural stability and higher capacity. DETAILED DESCRIPTION - Preparing metal sulfide/graphene involves adding graphene oxide in the ionic liquid, ultrasonically dispersing to obtain graphene oxide dispersion, adding the metal source to the graphene oxide dispersion, continuously ultrasonically dispersing to obtain the precursor. The sulfur source is added into the precursor to react at 150-220 degrees C for 8-20 hours, then the obtained product is washed, dried and calcined in tubular furnace in protection of inert atmosphere at 350-550 degrees C for 3-6 hours to obtain the metal sulfide/graphene, where the concentration of graphene oxide dispersion is 1-12 milligram/milliliter and the mass ratio of the metal source to the graphite oxide is 4:1-10:1.