• 专利标题:   Synthesizing three-dimensional electrode homogeneous polypyrrole nanowire array based on internal filtration flow comprises e. g. choosing three-dimensional material as electrode to build internal filtration synthesis device.
  • 专利号:   CN112940249-A, CN112940249-B
  • 发明人:   LIU H
  • 专利权人:   UNIV JINAN
  • 国际专利分类:   C08G073/06, H01G011/36, H01G011/86
  • 专利详细信息:   CN112940249-A 11 Jun 2021 C08G-073/06 202159 Pages: 9 Chinese
  • 申请详细信息:   CN112940249-A CN10119243 28 Jan 2021
  • 优先权号:   S, WANG Y, ZHANG J, WANG W, SUN M, LIANG CCN10119243

▎ 摘  要

NOVELTY - Synthesizing three-dimensional electrode homogeneous polypyrrole nanowire array based on internal filtration flow comprises (a) choosing a three-dimensional material as electrode to build internal filtration synthesis device, pumping the synthetic liquid from bottom to top into the electrode to filter the synthesis device, and forming a loop, connecting the anode and the first cathode of the device to the anode and cathode of the power supply respectively, starting the power supply, and reacting for 5-10 minutes; (b) changing the direction of water flow and change the position of the cathode, pumping the synthetic liquid from top to bottom into the electrode to filter the synthesis device, forming a loop, connecting the second cathode of the device to the negative pole of the power supply, starting the power supply, reacting for 5-10 minutes, and performing the above adjustments back and forth; and (c) stopping the device, taking out the anode material of the device. USE - The method is useful for synthesizing three-dimensional electrode homogeneous polypyrrole nanowire array based on internal filtration flow. ADVANTAGE - The method is simple and easy to control, and is suitable for generating homogeneous polypyrrole nanowire arrays on surface and inside of three-dimensional porous materials, and improves the application performance of polypyrrole nanowire. DETAILED DESCRIPTION - Synthesizing three-dimensional electrode homogeneous polypyrrole nanowire array based on internal filtration flow comprises (a) choosing a three-dimensional material as electrode to build internal filtration synthesis device, pumping the synthetic liquid from bottom to top into the electrode to filter the synthesis device, and forming a loop, connecting the anode and the first cathode of the device to the anode and cathode of the power supply respectively, starting the power supply, and reacting for 5-10 minutes; (b) changing the direction of water flow and change the position of the cathode, pumping the synthetic liquid from top to bottom into the electrode to filter the synthesis device, forming a loop, connecting the second cathode of the device to the negative pole of the power supply, starting the power supply, reacting for 5-10 minutes, and performing the above adjustments back and forth; and (c) stopping the device, taking out the anode material of the device and cleaning it with pure water to obtain three-dimensional electrode with homogeneous polypyrrole nanowire array on the surface and inside.